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勃姆石溶膠 / 偶氮染料混成材及其性質研究

指導老師：顏明賢 學號： 4960G003 學生： 賴威宇 日期： 100 年 1 月 8 日. 勃姆石溶膠 / 偶氮染料混成材及其性質研究.

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勃姆石溶膠 / 偶氮染料混成材及其性質研究

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  1. 指導老師：顏明賢 學號：4960G003 學生：賴威宇 日期：100年1月8日 勃姆石溶膠/偶氮染料混成材及其性質研究

  2. 本研究主要製備勃姆石溶膠(AlOOH)與噻唑偶氮染料之混成材料。先利用4-取代乙醯苯、硫代尿素及碘以隔水加熱迴流方式反應合成中間體4-取代2-胺基噻唑中間體並當作偶合鹽，分別與重氮鹽對硝基苯胺及對甲氧基苯胺反應，製得4-取代噻唑偶氮染料，進而將染料與不同比例的乙烯基三乙氧基矽烷(VTES)/異丙醇鋁(AIP)與VTES/四乙氧基矽烷(TEOS)/AIP產生水解聚縮合反應，製得VTES/ AlOOH和VTES/ TEOS/AlOOH與噻唑系偶氮染料之混成材料。再藉由FT-IR，29Si-NMR，SEM等儀器分析其化學結構。進而對聚醯胺織物進行染色加工，進而對各加工染織物探討其蓄熱保溫性、接觸角、耐磨擦、耐水洗堅牢度，透氣性與撥水度等各項物性。 摘要

  3. 謝謝各位評審聆聽!! Thanks for your attention!!

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