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Modular Sampling System Initiative Background and Status

Modular Sampling System Initiative Background and Status. 2000 Fall Sponsor Meeting Center for Process Analytical Chemistry. Agenda. Status and Update Preview of Swagelok Proposal. CPAC as a Multi-Purpose PA Forum. Legal Umbrella for Sponsors to Meet R&D: Long Range / Short Range

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Modular Sampling System Initiative Background and Status

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  1. Modular Sampling System InitiativeBackground and Status 2000 Fall Sponsor Meeting Center for Process Analytical Chemistry

  2. Agenda • Status and Update • Preview of Swagelok Proposal

  3. CPAC as a Multi-Purpose PA Forum • Legal Umbrella for Sponsors to Meet • R&D: Long Range / Short Range • Information Clearing House • Enabling Mechanism to Address Other Common Needs • Focus Groups: Forum to • Review R&D Programs • Present Industry Common Needs - RFP • Address Industry Common Needs • Fieldbus Datalink Specification - Done • NeSSI - In progress • MatLab On-line/Connectivity - Future?

  4. Background and Chronology of NeSSI Activities • O&P Focus Group May 1999 • Identified Sampling Systems as Common Area Of Interest • Sponsored Tutorial for Nov99 Sponsor Meeting • Tutorial Nov99 CPAC Meeting • Background/Reasons for Interest • Presentations by Suppliers/ End Users • Participation in IFPAC2000 Meeting • Plenary/General Papers (SS Enjoyed High Profile) • Workshop

  5. FLAN (Optical Fiber) Sensor = Moisture Probe P IA Controller (ASIC) F T A Sensor/Signal Bus Sampling System Vision

  6. Process Analyzer Vision

  7. Background and Chronology of NeSSI Activities (cnt’d) • Ad-hoc O&P Meeting @ Pittcon2000 • End-users Discuss Initial Target Designs • CPAC2000 Spring Meeting • Formed SS Focus Group • Defined Information Package (basis of RFP) • Distributed RFP (July 2000) • Clarification Meeting at ISAEXPO2000 (40 attendees) • Received Proposals from Swagelok, Parker • Expect Additional Proposals/Comments from Autoflow, ABB Analytical, SAAI, Rosemount Analytical

  8. Background and Chronology of NeSSI Activities (cnt’d) • CPAC2000 Fall Meeting • Preview of Swagelok Proposal • Other Feedback • Micro-Reactor Proposal (MicroAnalytics) • What is Next? • Distribute Proposals to All Interested Parties • Follow-up by Report • Sampling System Session at IFPAC2001 • Review and Summary of NeSSI Effort • Papers by Swagelok, Parker, Autoflow, ABB, Rosemount

  9. Acknowledgements • Dow Rob Dubois/Ron O’Reily/ Brian Worthington • Dow Corning Jim Tatera/Gary Bokerman • DuPont Bob Bucher • Rohm&Haas Joe Sung • Honeywell Ken Creasy • Akzo Nobel Foad Mozayeni • ExxonMobil Dan Podkulski/Rajko Puzic/ John Cumbus/Jeff Gunnell • Swagelok Dave Simko • CPAC Lloyd Burgess/Larry Ricker

  10. The End

  11. O&P Focus Group Meeting May 99 • Recognized Modular Sampling System Efforts in Semi Conductor Industry (Standard) • Vendors like Autoflow, A+, Swagelok etc. promoted modular designs • Recognized that current implementations of sample systems designs have not changed for many years • CPAC has promoted Versatile Micro Analytical Systems (VMAS) as a basis for future micro-analytical techniques • O&P decided to sponsor a SSISSS (Small Smart Integrated Sensor and Sampling System) Tutorial at CPAC Nov Meeting

  12. Nov99 CPAC SSISSS Tutorial • ExxonMobil/DuPont Provided Introduction to Tutorial • Validation of Sample System Performance • Integration of Sensor with Sampling System • Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: • A+, Autoflow, Swagelok, Rosemount • Many components commercially Available • GCX example of self-contained miniaturized GC (GC on a pole) • Recognition • Modular Sampling System can be a platform to integrate VMAS • Bridge between Process Sample (Macro world) Micro Fluidics Sensors/Analyzers

  13. Driving Forces for Change • Reduce Cost of Ownership • Non Recurring Costs = Cost to Build • Operating Cost • Data Validation (Fit for Use)

  14. Integration of Sample System and Sensors A Field LAN P Analyzer Controller T Sample Conditioning System F Mainly a Trust Configuration Now a Trust & Verify Configuration All System Components in Contact with Sample including the Sensors Process Stream All Additional Electronic and Computing Components Required to Generate Analytical Result Level 1 Level 0

  15. Level 0 Subsystem Integration A P Integrated Sampling/Sensor System T Sample Conditioning System F Purpose: Prepare and Verify a Representative Sample (Compatible with Analyzer Sensor) • Opportunity: • Packaging as an Integrated Sensor and Sampling System • Size • Cost Process Stream • Issues: • Size • Standardization • VMAS Level 0

  16. Separation or Integration of Level 0/1 Subsystems A Field LAN P Analyzer Controller T F Objective: Close to Sample Tap Process Stream Integrated Sampling/Sensor System Options: • Remote • Separate but Close • Integrated Level 1 Level 0

  17. Integration of Level 0/1 Subsystems Integrated Sampling/Sensor/Controller System A Field LAN P Analyzer Controller T F Process Stream $$ Level 1 Level 0

  18. Nov99 CPAC SSISSS Tutorial • ExxonMobil/DuPont Provided Introduction to Tutorial • Validation of Sample System Performance • Integration of Sensor with Sampling System • Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: • A+, Autoflow, Swagelok, Rosemount • Many components commercially Available • GCX example of self-contained miniaturized GC (GC on a pole) • Recognition • Modular Sampling System can be a platform to integrate VMAS • Bridge between Process Sample (Macro world) Micro Fluidics Sensors/Analyzers

  19. Nov99 CPAC SSISSS Tutorial (Vendor Presentations) Swagelok Autoflow A+ Rosemount

  20. Nov99 CPAC SSISSS Tutorial • ExxonMobil/DuPont Provided Introduction to Tutorial • Validation of Sample System Performance • Integration of Sensor with Sampling System • Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: • A+, Autoflow, Swagelok, Rosemount • Many components commercially Available • GCX example of self-contained miniaturized GC (GC on a pole) • Recognition • Modular Sampling System can be a platform to integrate VMAS • Bridge between Process Sample (Macro world) and Micro Fluidics Sensors/Analyzers

  21. IFPAC2000 • ExxonMobil Presented Plenary Paper Promoting SSISSS • Sample System Infrastructure accounts for 50+% Cost to Build • Proposed Conceptual Design for SSISSS • Highlighted sensor and analyzer transmitter configurations • Sampling System Session • Presentations by A+, Autoflow, etc. • Sampling Systems enjoyed a High Profile • CPAC/ExxonMobil sponsored Workshop • Confirmed high interest in Modular Sampling System • Provided input for the ISA Standardization effort

  22. For a major greenfield project TODAY’S COST OF BUILD

  23. TODAY’S COST OF OWNERSHIP

  24. Field LAN IMAGINE THE FUTURE A P Process Stream Analyzer Controller T F Level 1 Level 0

  25. IMAGINE THE FUTURE FLAN (Optical Fiber) Sensor = Moisture Probe P IA Controller(ASIC) & Interface Module F T A Sensor/Signal Bus Original Picture of Gas Delivery System courtesy Valin Corporation;

  26. IMAGINE THE FUTURE Sensor = RAMAN Probe P F Interface Module T A

  27. IFPAC2000 • ExxonMobil Presented Plenary Paper Promoting SSISSS • Sample System Infrastructure accounts for 50+% Cost to Build • Proposed Conceptual Design fro SSISSS • Highlighted sensor and analyzer transmitter configurations • Sampling System Session • Presentations by A+, Autoflow, etc. • Sampling Systems enjoyed a High Profile • CPAC/ExxonMobil sponsored Workshop • Confirmed high interest in Modular Sampling System • Provided input for the ISA Standardization effort

  28. IFPAC2000 • ExxonMobil Presented Plenary Paper Promoting SSISSS • Sample System Infrastructure accounts for 50+% Cost to Build • Proposed Conceptual Design fro SSISSS • Highlighted sensor and analyzer transmitter configurations • Sampling System Session • Presentations by A+, Autoflow, etc. • Sampling Systems enjoyed a High Profile • CPAC/ExxonMobil sponsored Workshop • Confirmed high interest in Modular Sampling System • Provided input for the ISA Standardization effort

  29. Pittcon2000 (New Orleans) • O&P Ad-Hoc Meeting of Sponsor End-users • DuPont, Dow, Dow-Corning, CPAC, Rohm&Haas, ExxonMobil • Main Goal: Identify Typical Sample System Designs as Candidates for Modular Design • Reviewed some typical gas/liquid sample System Designs • Rob DuBois Presented a Modular Component/Service Matrix • Discussed next steps • Present Sample System Data at May CPAC Meeting • Next Step is to Open Up Discussion (3rd parties) • Leverage ISA Meeting in New Orleans (Aug00) • Role of CPAC in Facilitating Development/Testing of a Prototype System • Larry Ricker/Lloyd Burgess to Present Proposal

  30. Status • CPAC Meeting May 1999 Done • O&P Identified Modular Sampling Systems • CPAC Meeting Nov 1999 Done • O&P Sponsored Tutorial • IFPAC2000 MeetingDone • Plenary Presentation Promoted SSISS • Session on Modular Sampling Systems • CPAC Sponsored Workshop • Pittcon2000Done • Ad-hoc O&P Meeting • Propose Candidate Sampling System Descriptions • CPAC Meeting May 2000 TBD

  31. What is Next? • CPAC Meeting May 2000 (Sampling Focus Group – Wednesday) • Review and Agree on Sample System Information Package • Involvement of 3rd parties • How do we distribute package (Distribution List, Meeting?) • Expectations for proposals from Suppliers (Paper designs?) • Joint Effort with ISA (Meeting in Aug, New Orleans) • Evaluation of Designs - Recommendation • Prototype design/manufacturing/testing at CPAC • Larry Ricker/Lloyd Burgess proposal • Program to Evaluate Test Platforms fro Micro Analytical Devices • CPAC Proposal – Lloyd Burgess

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