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Eric D. Isaacs CNM Director February 23, 2004

Center for Nanoscale Materials Overview. Basic Energy Sciences Advisory Committee Nanoscience Research Center Review. Eric D. Isaacs CNM Director February 23, 2004. Argonne National Laboratory. A U.S. Department of Energy Office of Science Laboratory Operated by The University of Chicago.

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Eric D. Isaacs CNM Director February 23, 2004

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  1. Center for Nanoscale Materials Overview Basic Energy Sciences Advisory Committee Nanoscience Research Center Review Eric D. Isaacs CNM Director February 23, 2004 Argonne National Laboratory A U.S. Department of EnergyOffice of Science Laboratory Operated by The University of Chicago BESAC NSRC Review February, 23, 2003

  2. Talk Overview • Introduction to the Center for Nanoscale Materials. • Scientific themes. • Technical capabilities. • X-ray nanoprobe. • Path to Operations • User science and outreach programs • Jumpstart BESAC NSRC Review February, 23, 2003

  3. Center for Nanoscale Materials • World-class research facility at • Argonne National Laboratory for tackling the grand challenges of nanoscience. • $36 M DOE equipment funds. • $36 M State-of-Illinois funds. • Building completed in FY06. • $18.5 M DOE operations funds • in FY07. $ 72 M Federal/State Partnership BESAC NSRC Review February, 23, 2003

  4. To explore novel phenomena associated with the interplay between spatial, physical and chemical length scales and proximity effects.To transform the art of nanomaterial and nanodevice fabrication into a science.To characterize the 3D structural, electronic, magnetic and chemical properties of a single nanoparticle.To lay foundations for new technologies based on the principles of nanoscience. Global Nanoscience Challenges BESAC NSRC Review February, 23, 2003

  5. CNM Scientific Themes • bio-inorganic interface (D. Tiede, T. Rajh, CHM) • nanocarbon (D. Gruen, J. Carlisle, MSD) • nanomagnetism (S. Bader, A. Hoffman, MSD) • complex oxides (O. Auciello, S. Streiffer, MSD) • nanophotonics (G. Wiederrecht, CHM) • Virtual Fab Lab (S. Gray, CHM and P. Zapol, MSD) • X-ray Nanoprobe (B. Stephenson, MSD, J. Maser) Novel functional nanocomposites Self-assembled, functionalized arrays Sub-wavelength photon confinement/propagation BESAC NSRC Review February, 23, 2003

  6. Center for Nanoscale Materials Principals • World-class research facility for tackling the grand challenges of nanoscience, transforming the art of nanomaterials and nanodevices to a science. • Open access for all users. • best science via peer review (http://nano.anl.gov). • Bringing new science and capabilities to ANL, the region and the nation. • Leveraging Argonne’s and regional strengths. • One-stop access to BES facilities at Argonne: Advanced Photon Source, Intense Pulsed Neutron Source, Electron Microscopy Center. • Complements four other BES NSRC’s. BESAC NSRC Review February, 23, 2003

  7. Apertureless NSOM Enabling Science through Technical Capabilities CNM experimental themes share common technical activities: Synthesis • Self-assembly (chemical, electrochemical, size-selected nanoparticles etc.) • Thin film synthesis Sculpting • Nanolithography • Milling and etching Characterization • Investigate the synthetic process • Explore chemistry, physics, materials structure & properties Theory and Simulation • Leverage resources from ANL’s petaflop initiatives and DOE/SC computing infrastructure investment Aligned Polymer Scaffolds BESAC NSRC Review February, 23, 2003

  8. 1000 nm 1 100 nm 2 10 nm 3 ‘Assisted’ Self-Assembly Cross-Cuts Many Themes in Nanoscience and the CNM Stage 1: Substrate with lithographically prepared trenches Stage 2: Self-assembled diblock copolymer aligning within the trenches Stage 3: 1-D nanomag array selectively adsorbs on hydrophobic polymer stripes Darling, Lin, Bader (ANL) Sibener, Jaeger (U of C) Mirkin, Stupp (NU) Example: Beyond GMR (> 5Mb/cm2) Fe(CO)5 + Pt(acac)2→ FePt BESAC NSRC Review February, 23, 2003

  9. LEO 1560XB CrossBeam Key Fabrication and Characterization Tools Plasma-enhanced CVD for carbon FIB/SEM e-beam lithography combined SEM/SPM BESAC NSRC Review February, 23, 2003

  10. The Center for Nanoscale MaterialsHard X-ray Nanoprobe • Unique, versatile instrument to study individual nanostructures (30 nm resolution). • Quantitative atomic-scale structure, strain, orientation and imaging. • Sensitive trace element and chemical state analysis. • Operates in both scanning probe and full field. • Future: combine hard/soft x-ray microscopy. BESAC NSRC Review February, 23, 2003

  11. Grand Challenges for Nanoscience with X-rays • X-ray wavelength resolution. • 3D structural, chemical, electronic and magnetic properties at the nanoscale. • Structure of single macromolecule. • Dynamics of single nanoparticle. • Coherent manipulation of nanoparticles (LCLS). • Nonlinear x-ray processes (LCLS). BESAC NSRC Review February, 23, 2003

  12. data 10 m Hard X-ray Imaging at the Nanoscale Hard x-ray scanning probe Coherent Diffraction inversion absolute electron density Antiferromagnetic domains in chromium Evans, Isaacs, Aeppli, Lai & Cai, Science295, 1042 (2002). e-coli bacteria Miao, Hodgson, et al., Proc. Natl. Acad. Sci. USA,100, 110 (2003). BESAC NSRC Review February, 23, 2003

  13. Facilities Beyond CNM…. • DOE BES User Facilities at Argonne • The Advanced Photon Source, Intense Pulsed Neutron Source, Electron Microscopy Center • ‘one-stop’ user access to all four • DOE’s other NSRCs • The Center for Nanophase Materials Sciences, The Molecular Foundry, The Center for Functional Nanomaterials, The Center for Integrated Nanotechnologies BESAC NSRC Review February, 23, 2003

  14. Center for Nanoscale Materials Building • Adjacent to APS Sector 26 • Integrated with APS site design • Utilize APS site utilities BESAC NSRC Review February, 23, 2003

  15. Center for Nanoscale Materials Building ~85,000 gross square feet, including: • 13,000 sq ft Laboratories • 11,000 sq ft Cleanroom Facilities • 33,000 sq ft Offices & Public Spaces BESAC NSRC Review February, 23, 2003

  16. Public Space & Offices Cleanrooms Laboratories Support Center for Nanoscale Materials Building X-ray Nanoprobe Beamline BESAC NSRC Review February, 23, 2003

  17. CNM Operations Mission: Supporting users in doing outstanding science in a safe environment. Enabling world-class nanoscience aligned with DOE’s scientific mission. BESAC NSRC Review February, 23, 2003

  18. CNM Operations – Challenges • Maintaining a balance between User support and CNM science. • Technical support for User science. • Scientific leadership driving the future vision for CNM. • Staffing CNM with technical support to provide our Users with the highest quality support and to take full advantage of phased operations schedule. BESAC NSRC Review February, 23, 2003

  19. Equipment Cost/Schedule -Phased Operations Plan phased ops (CD-4) Project complete, begin full ops Accept nanoprobe Accept 10th piece of tech. equipment Dollars (cumulative to date) Accept building, initial ops begin Earliest install, Hoods Accept 1st piece of tech. equipment Start nanoprobe construction Start building construction, place HVEBL contract Start equipment procurement Oct 03 Apr 04 Oct 04 Apr 05 Oct 05 Apr 06 Oct 06 Apr 07 Oct 07 BESAC NSRC Review February, 23, 2003

  20. CNM Operations Funding Profile – Phased Operations CD-4b, full ops begin CD-4a Funding ($ M) Year BESAC NSRC Review February, 23, 2003

  21. Projected CNM Staffing – Overview FTE Includes 12 post docs and six lead scientists in FY08. Year Goal: full staffing by FY08 (2.5 years !) BESAC NSRC Review February, 23, 2003

  22. Estimated CNM User Visits Estimated User Visits (per month) Year BESAC NSRC Review February, 23, 2003

  23. Example: Nanolithography User Activity Projections • CNM cleanroom user activities • Lithography, Wet Chemistry, Synthesis • 140 per month in FY06 • 220 per month in FY09 • Tool increase by FY09 needed to satisfy demand • Existing low-voltage ebeam tool at ANL has ~ 30 user visits/month average. BESAC NSRC Review February, 23, 2003

  24. Building the Foundations for a CNM User Community • Universities to play critical role in CNM. • Nanoscience Workshops • Northwestern (Oct.’03); Notre Dame (Jan.’04); U. of Mich. (Spring ’04); EPSCoR States (June ’04),…. • Joint hires w/regional Universities – U of C, NU, UIC, … • Consortium for Nanoscience Research. • Joint ANL/U of C Institute – H. Jaeger, Dir., S. Bader, Deputy Dir. • Scientific Theme/Technical Workshops. • 1st CNM User Meeting, May 3 – 4, 2004. • Developing a vision for the ‘Ultimate X-ray Microscope’. • Planning workshop at ANL in June ‘04. BESAC NSRC Review February, 23, 2003

  25. Jumpstart Funding for CNM Science • Jumpstart funds – $1.5M (FY03). • CNM Post-doc fellow program (user outreach). • Alex Bouhelier – nanoplasmonics/photonics • Andrew Goshe – nanobiomaterials • Amanda Barnard – theory and modeling (Virtual Fab Lab) • Oliver Williams – nano-crystalline diamond • Yi Ji – nanomagnetism • Dolly Batra – bio-inorganic interfaces • Add three more post-docs in FY04 • High resolution e-beam lithography (ANL tool purchase). • Leo Ocola - Raith 150, 25 kV, JEOL, 100 kV (@ Bell Labs). • User Program/Access. • Nena Moonier, User coordinator to start Feb. ’04 (50% APS). • Xiao-min Lin, website (50% MSD/CHM) • Nanoscience Summer School 2003. BESAC NSRC Review February, 23, 2003

  26. Nanoscience & Health • Risk assessment • Risk (cost) = Σ(severity of effects x probability of effects) + public perception. • Environmental & Workers Health Concerns. • Physiology meets anatomy. • Control technologies available (e.g., equipment & procedures for bio-hazards level 2). • Public relations • Following literature. • Community forums (e.g., CNM building title II review). • Opportunities • Collaborating with other NSRC’s. • Networking with researchers (e.g., A. Maynard, NIOSH). • Support research. BESAC NSRC Review February, 23, 2003

  27. Center for Nanoscale Materials Project Organization DOE Associate Director, BES P.M. Dehmer, Acquisition Executive for MIE DOE CH – Argonne Area Office R. Wunderlich, Acquisition Executive for CNM building DOE NSRC Program Manager K. Bennett CNM Federal Project Director F. Gines Scientific Advisory Committee E. Hu and R. Buhrman CENTER FOR NANOSCALE MATERIALS E. Isaacs, Director CNM Project D. Mancini, Project Manager Project Advisory Committee Dale Knutson, Chair Scientific Theme Leaders & Stakeholders Bionanocomposites, Nanomagnetism, Nanophotonics, Nanocarbon, Complex oxides, Virtual Fab Lab Exec. Secretary, S. Gunter-Harris Assist. Division Director, J. Morgenthaler User Coordinator, N. Moonier ES&H Coordinator, B. Stockmeier WBS 1.1 Nanoprobe B. Stephenson WBS 1.2 Nanolithography and Processing L. Ocola WBS 1.3 Nanosynthesis and Characterization S. Streiffer WBS 1.4 Project Management, Integration & Infrastr. D. Mancini WBS 1.5 Conventional Facilities K. Hellman BESAC NSRC Review February, 23, 2003

  28. Center for Nanoscale Materials Participants Scientific Theme Leaders Orlando Auciello Sam Bader John Carlisle Millie Firestone Stephen Gray Dieter Gruen Axel Hoffman Jorg Maser Tijana Rajh Brian Stephenson Stephen Streiffer David Tiede Gary Wiederrecht Peter Zapol ANL Project Team Leaders Derrick Mancini Stephen Streiffer Brian Stephenson Leo Ocola Karen Hellman Sam Bader (Bev Hartline) DOE Kristin Bennett Tof Carim Pat Dehmer Frank Gines Helen Kerch Pedro Montano Bill Oosterhuis Robert Wunderlich Other Key Participants George Crabtree Murray Gibson Efim Gluskin Heinrich Jaeger, U of C Dale Knutson Gabrielle Long Lee Makowski Bob Rosner Steve Sibener, U of C Al Wagner BESAC NSRC Review February, 23, 2003

  29. CNM Scientific Advisory Committee • Charter: Reports to Argonne Director, providing science and policy advice at the highest level • Reviews & advises on scientific themes & technical equipment plans • First meeting May 2003 • Next meeting planned for Spring 2004. • Membership • Robert Buhrman (Co-chair), Cornell University • Evelyn Hu (Co-chair), University of California Santa Barbara • Federico Capasso, Harvard University (previously with Lucent) • Daniel Chemla, Univ. Calif. Berkeley, Lawrence Berkeley National Lab • Vicki Colvin, Rice University • Heinrich Jaeger, University of Chicago • Barbara Jones, IBM Almaden Research Center • Janos Kirz, State University of New York, Stony Brook • Samuel Stupp, Northwestern University Currently updating SAC to include biophysicist/chemist BESAC NSRC Review February, 23, 2003

  30. Center for Nanoscale Materials • World-class research facility at • Argonne for tackling the • grand challenges of nanoscience. • transforming the art of nanomaterials to a science. • 3D properties of a single nanoparticle. • laying the foundations for future nanotechnologies. $ 72 M Federal/State Partnership BESAC NSRC Review February, 23, 2003

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