120 likes | 308 Views
volume dilatometry. moisture / temperature. time / rate. dielectrometry. longitudinal / transverse strain. laser extensometry. videothermography. crack-opening displacement. load-line displacement. ultrasonic analysis. load / stress. acoustic emission analysis. parameters. sensors.
E N D
volume dilatometry moisture / temperature time / rate dielectrometry longitudinal / transverse strain laser extensometry videothermography crack-opening displacement load-line displacement ultrasonic analysis load / stress acoustic emission analysis parameters sensors in-situ methods material parameters damage and failure criteria morphology characterization morphology - property - correlations defectoscopy material optimization component monitoring Fig.: 9.1 Chapter 9: Bierögel, C.: Hybrid Methods of Polymer Diagnostics. In: Grellmann, W., Seidler, S. (Eds.): Polymer Testing. Carl Hanser Verlag, Munich (2013) 2. Edition
AE analyzer oscilloscope AE signal F Power HDD PW Mouse Keyboard AE sensor ASMY4-CP ASMY4-PC preamplifier preamplifier infrared camera thermotracer F ON Step COL TR RUN ISO F1 SH GPIB Multi Wave FRZ Mode Page F2 CM Power F3 Sens Level Auto F F4 CR Time Focu Zoom I O ENT CA Rang Emis CAL nbn-Thermo-Tracer 6 T62 tripod Color-Monitor I/O CT specimen F Fig.: 9.2 Chapter 9: Bierögel, C.: Hybrid Methods of Polymer Diagnostics. In: Grellmann, W., Seidler, S. (Eds.): Polymer Testing. Carl Hanser Verlag, Munich (2013) 2. Edition
26.1 25.7 25.3 24.9 24.5 24.1 23.7 23.3 22.9 22.4 22.0 21.6 21.2 20.8 20.4 20.0 19.6 1000 e TE 40 800 e AE -1 De 30 600 . s (MPa) hits s 20 400 10 200 0 0 1.5 3.0 4.5 6.0 7.5 0 1.8 4.9 7.4 e (%) e (%) T (°C) i i Fig.: 9.3 Chapter 9: Bierögel, C.: Hybrid Methods of Polymer Diagnostics. In: Grellmann, W., Seidler, S. (Eds.): Polymer Testing. Carl Hanser Verlag, Munich (2013) 2. Edition
scan direction specimen with reflectors 50 40 e (%) 30 l laser laser beam 20 t (s) 10 cylinder lens 10 0 rotating mirror 8 start 6 zones 4 2 stop 0 1 20 25 5 10 15 collecting lens photodiode evaluation, results and graphics Fig.: 9.4 Chapter 9: Bierögel, C.: Hybrid Methods of Polymer Diagnostics. In: Grellmann, W., Seidler, S. (Eds.): Polymer Testing. Carl Hanser Verlag, Munich (2013) 2. Edition
b a local e (%) e (%) integral e l max e i e e l l min t (s) t (s) 1 d c s(e ) initiation region s (MPa) l l min max H/H s(e ) i i s(e ) l l max minimum heterogenity valid values of heterogenity 0 e (%) e (%) i Fig.: 9.5 Chapter 9: Bierögel, C.: Hybrid Methods of Polymer Diagnostics. In: Grellmann, W., Seidler, S. (Eds.): Polymer Testing. Carl Hanser Verlag, Munich (2013) 2. Edition
8 8 900 300 240 720 6 6 e (%) e (%) 540 180 l l 4 4 360 120 t (s) t (s) 2 2 60 180 0 0 0 0 32 32 1 1 24 24 16 16 8 8 reflector fringes reflector fringes Fig.: 9.6 Chapter 9: Bierögel, C.: Hybrid Methods of Polymer Diagnostics. In: Grellmann, W., Seidler, S. (Eds.): Polymer Testing. Carl Hanser Verlag, Munich (2013) 2. Edition
PA 10 PA 30 12 200 10 160 8 e (%) 120 6 l 80 t (s) 4 2 40 0 0 1 5 7 9 3 11 13 local region PA 10 PA 30 weld welding region Fig.: 9.7 Chapter 9: Bierögel, C.: Hybrid Methods of Polymer Diagnostics. In: Grellmann, W., Seidler, S. (Eds.): Polymer Testing. Carl Hanser Verlag, Munich (2013) 2. Edition
scan direction laser array 123456 specimen with reflectors laser beam cylinder lens start rotating mirror stop collecting lens photodiode evaluation, results and graphics Fig.: 9.8 Chapter 9: Bierögel, C.: Hybrid Methods of Polymer Diagnostics. In: Grellmann, W., Seidler, S. (Eds.): Polymer Testing. Carl Hanser Verlag, Munich (2013) 2. Edition
b a e(%) e(%) e(%) e(%) l l l l e = 6 % e = 2 % i i 20 20 20 20 6 6 scan scan 10 10 10 10 1 1 32 1 reflector fringes 32 1 reflector fringes 0 0 0 0 c d e = 8 % e = 10 % i i 6 6 scan scan 1 1 32 1 32 reflector fringes 1 reflector fringes e 6 F F 1 1 32 scan 65 25 105 Fig.: 9.9 Chapter 9: Bierögel, C.: Hybrid Methods of Polymer Diagnostics. In: Grellmann, W., Seidler, S. (Eds.): Polymer Testing. Carl Hanser Verlag, Munich (2013) 2. Edition
d b a microscope Da support digital camera specimen bending punch 500 µm 1.5 c blunting Line 1.0 d (mm) 0.5 crack growth curve d i 0 0 0.1 0.2 0.3 0.4 0.5 0.6 Da Da (mm) SZW Fig.: 9.10 Chapter 9: Bierögel, C.: Hybrid Methods of Polymer Diagnostics. In: Grellmann, W., Seidler, S. (Eds.): Polymer Testing. Carl Hanser Verlag, Munich (2013) 2. Edition
a 1 2 3 4 5 6 7 8 9 crack opening 0 30 75 120 150 180 210 240 257 t (s) 60 80 c b 50 phr 40 phr 60 9 30 phr 40 8 7 J (N mm-1) J (N mm-1) 6 5 40 4 15 phr 3 2 20 1 20 crack initiation 0 phr 0 0 0 5 10 15 20 25 30 35 0 5 10 15 20 25 crack opening (mm) crack opening (mm) Fig.: 9.11 Chapter 9: Bierögel, C.: Hybrid Methods of Polymer Diagnostics. In: Grellmann, W., Seidler, S. (Eds.): Polymer Testing. Carl Hanser Verlag, Munich (2013) 2. Edition
specimen 400 F (t) F 10 300 AE waveform 5 AE level (V) load (N) 200 0 AE sensor -5 100 stable (t , F) i i e AE sensor R -10 0 laser beam 0 200 600 1000 1400 400 1200 800 COD time (µs) Fig.: 9.12 Chapter 9: Bierögel, C.: Hybrid Methods of Polymer Diagnostics. In: Grellmann, W., Seidler, S. (Eds.): Polymer Testing. Carl Hanser Verlag, Munich (2013) 2. Edition