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Microstructure Evolution of Semi-solid Magnesium Alloy AZ91D Under Electric Current. Y Yang , Q Zhou, J Tang, Z Hu Institute of Metal Research Chinese Academy of Sciences. 2ed Sino-German Workshop on EPM, 16-19 Oct. 2005, Dresden, Germany. Outline. Introduction Experimental procedure
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Microstructure Evolution of Semi-solid Magnesium Alloy AZ91D Under Electric Current Y Yang, Q Zhou, J Tang, Z Hu Institute of Metal Research Chinese Academy of Sciences 2ed Sino-German Workshop on EPM, 16-19 Oct. 2005, Dresden, Germany
Outline • Introduction • Experimental procedure • Results • Dendritic growth • Current pulse density • Current pulse duration • Discharging cycle • Treating time • Nondendritic particle size • Thermal fluctuation • Conclusions
The most lightest structural alloy • Anti-vibration Introduction • Magnesium alloy offers numerous merits in physical, mechanical and casting properties.
Usages of magnesium alloy • Magnesium alloy to near-netshape will find widespread application in auto-, video-, computer- and communication- equipment, combined with the on-going ‘light-weighting’ of components.
Dendrites in AZ91D solidified with Low-Voltage Electric Current Pulses method (LVECP)
Experimental Schematics of experimental setup
density time duration discharging cycle Pulse current density curve • Parameters: • Current pulse density: 0, 1.3, 3, 4.3, 5.2 kA/cm2 • Current pulse duration: 0, 0.6, 1.0, 1.2, 1.5 ms • Discharging cycle: 0, 4, 6, 8, 10, 12 sec • Treating time: 0, 5, 10, 15, 20 min
Experimental Material Compositions of the AZ91D alloy (wt.%) Commercial AZ91D alloy Liquidus temperature: 595 oC Solidus temperature: 470 oC
1 kA/cm2 3 kA/cm2 4 kA/cm2 5 kA/cm2 Effect of current pulse density on dendrite growth (a) Big dendrites; (b) small dendrites; (c) globular and cosh-shaped. (d) nondendritic, equiaxed paticles.
0.6 ms 1.0 ms 1.2 ms 1.5 ms Effect of current durationon dendrite growth (a) Dendrites with long primary arms; (b, c) rosette-shaped. (d) globular and cosh-shaped.
6 sec 8 sec 10 sec 12 sec Effect of discharging cycle on dendrite growth (a) globular and cosh-shaped; (b, c) rosette-shaped; (d) dendritic structure.
5min 10min 15min 20min Effect of treating time on dendrite growth The shape of the primary grains from dendritic to rosette-shaped then nondendritic with increasing treating time.
Distribution of non-dendritic particle size The average size of the particles is about 150 m
Thermal fluctuation during solidification • Thermal history of specimen The temperature of the sample with current pulse treatment is higher after treating time exceeds 20 minutes due to Joule heating. • Temperature fluctuation The temperature fluctuation increases as the current density increases. The maximal temperature fluctuation is about 16 oC.
Schematic illustration of dendrite evolution (a) initial dendritic (b) shrinkage of secondary arm roots (c) remelting and detaching of secondary arm roots (d) detaching finished
Conclusions • The morphology of primary phase is transited from dendritic to nondendritic, equiaxed particles by Low-voltage Electric Current Pulses during solidification of AZ91D alloy. • The particle size of AZ91D alloy decreases with increase of the current pulse density, discharging cycle, and treating time; but increases with increasing the current pulse duration. • Heat generation caused by Joule heating during discharge causes temperature fluctuation and decreases the cooling rate of solidification. • Electric current pulse restrains growth of the dendrites, makes dendrite arms remelted and attached during solidification, which leads to formation of nondendritic, equiaxed structure.