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Microstructure. MENA3100,OBK, 18.01.12. Based on chapter 1. The Consept of Microstructure. Microstructural morphology Microanalysis Crystal structure. How?. Interaction between sample and. light. X-rays. electrones. neutrons. + SPM. Image. Spectrum. Diffraction pattern.
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Microstructure MENA3100,OBK, 18.01.12
Based on chapter 1 The Consept of Microstructure
Microstructural morphology Microanalysis Crystal structure
How? Interaction between sample and light X-rays electrones neutrons + SPM Image Spectrum Diffraction pattern
Optical microscopy Electron microscopy Scanning electron microscopy (SEM) Transmission electron microscopy (TEM) Diffraction X-ray diffraction (XRD) Electron diffraction Neutron diffraction X-ray spectroscopy Energy dispersive spectroscopy (EDS) Wavelength dispersive spectroscopy Auger electron microscopy X-ray photo spectroscopy (XPS) Electron energy loss spectroscopy (EELS) Scanning probe microscopy (SPM) Atomic force microscopy (AFM) Scanning tunneling microscopy (STM) SEM
Why? Is microstructure important? Well ... Structure-insensitive Structure-sensitive Young’s modulus Yield strength Thermal expansion coeffisient Thermal conductivity Specific gravity Electrical resistivity
”Mikrostruktur” s. 10 Makrostruktur Mesostruktur Mikrostruktur Nanostruktur
Calcite Marble Granite A crystal Monocrystalline Polycrystalline Multiphase
Crystals can be: Equidimensional Acicular Tabular ...
Measure size Caliper diameter ASTM Grain-size Chart DA = NA-1/2 DL = NL-1
Crystallography Enhetscelle Gitter + basis
Crystal system Axial system Bravais lattice Point group Space group
7 Crystal system
7 Crystal system