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Structure , goalS & CURRENT STATUS

Giorgos Stefanidis. Structure , goalS & CURRENT STATUS. 2nd Consortium M eeting Amersfoort, 8.7.2013. Current status . Project started 01.01.2013. F irst six months completed .

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Structure , goalS & CURRENT STATUS

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  1. Giorgos Stefanidis Structure, goalS & CURRENT STATUS 2nd ConsortiumMeeting Amersfoort, 8.7.2013

  2. Current status • Project started 01.01.2013. First sixmonthscompleted. • Subprojects (WPs) havebeenstaffed. First stepstowardsmeetingthefirstdeliverablecommittmentshavebeenmade. • First biannualtechnicalreporttobesenttothe Project officerwithin 2 weeks • Nofinancialissues • Consortiumagreement: feedbackhasbeenreceivedbysomepartners. An updaredversion will besentbythe TUD contractmanagertothepartnersforapproval.

  3. General concept “The general aim of the project is to develop a hierarchical methodology for targeted supply of three alternative forms of energy (ultrasound, plasma and microwaves) in novel integrated reactors to precisely control chemical transformations and reaction pathways. It is based on fundamental mechanism understanding, advanced modeling, experimentation, and model validation. An anticipated groundbreaking solution will consist in creating a reaction environment in which the right type of energy is transferred selectively from the source to the target molecules in the required form, in the required amount, at the required moment, and at the required position.”

  4. Advanced pharmaceutical synthesis Green fuel synthesis Technologies General work plan TUDO TUD YORK SAIREM JP KUL TUD TUDO JP SM TUD AN SAIREM JP KUL TUD SAIREM Ultrasound Microwaves Ultrasound Plasma Demonstration Application areas WP 4 AN TUDO TUD SAIREM SM WP 5 WP 1 WP 2 WP 3 Data generation Mechanisms and models Equipment design and scale up 30.01.2013

  5. Fuelsand Pharmaceuticals Syntheses • Methanol from CO2 hydrogenation and syngas from biomass gasification activated by (microwave) plasma. • Ethyl methyl carbonate (EMC) and Diethyl carbonate (DEC) from transesterification of DMC with ethanol via reactive distillation activated by microwaves. Effect of US on VLE. • API synthesis in millireactors activated by microwaves (some chemistries have been suggested by JM) • Paracetamolsynthesis in millireactors and OFRs assisted by ultrasound and microwaves • Reactive extraction in biphasic water/toluene (other solvent) systems assisted by ultrasound 30.01.2013

  6. st nd rd th 1 year 2 year 3 year 4 year Research & Technical Development Demonstration Equipment implementation & Equipment Experimentation for Data set Generation Model Development Design & Process Evaluation Development ALTEREGO Workflow Schedule

  7. First Deliverables • WP1: Month 12 (Report) • Complete set of data for comparison between US and non-US processes and for input to modeling. • WP2: Month 12 (Report) • Complete set of thermodynamic and kinetic data. • WP3: Month 15 (prototype) • Small scale microwave plasma (catalytic) reactor integrated with process analytics tools. • WP7: Every 6 months (report) • Biannual report 30.01.2013

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