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Superconductor/Manganite Bilayer Thin Films in Cross Section. Isaac Brown 2003-04. Introduction. Smooth Cross Sections Materials Ceramic Superconductor: DyBa 2 Cu 3 O 7 Substrate: SrTiO 3 Manganite: La 2/3 Ba 1/3 MnO 3 Doped: LaMnO 3. Applications. •Electromagnets Power
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Superconductor/Manganite Bilayer Thin Films in Cross Section Isaac Brown 2003-04
Introduction • Smooth Cross Sections • Materials • Ceramic Superconductor: DyBa2Cu3O7 • Substrate: SrTiO3 • Manganite: La2/3Ba1/3MnO3 • Doped: LaMnO3
Applications • •Electromagnets • Power – Generation – Transportation • Switching Devices
Method 1: Sandblaster • Thinned substrate from the back with sandblaster • Desired thickness after sandblasting: 50 µm • Snapped thinned sample
Method 2: Polisher • Polished fragment with diamond sandpaper • Lubricated with • Water • Glycerol
Method 3: Microtome • Embeded fragment in epoxy • Cut off thin slices with glass knife
Measurements: AFM Height • Measured height with an atomic force microscope • Used 3 µm by 3 µm areas • Took root mean squared roughness readings on full area and facets • Desired value: 30 Å or less
Measurements: AFM Friction • Took readings of relative friction so that different materials are distinctly visible • Used to verify film quality and ability to be imaged
Discussion: Facets • Facet size does not affect facet RMS roughness • Overall RMS roughness does not affect facet RMS roughness • Facets are not arbitrary
Discussion: Methods • Microtomy, using facets, was the smoothest usable method • A film was imaged from only from one microtomy sample • Epoxy and substrate should be minimized to protect film during microtomy
What Is Next? • Scanning Tunneling Microscope • Spin-polarized current • Structure • Supercondutor switching devices using the bilayer
Acknowledgements • Dr. Goldman • Ms. Fruen • Research class • Everybody from the Goldman lab
Superconductor/Manganite Bilayer Thin Films in Cross Section Isaac Brown 2003-04