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Flowchart for the Laboratory. Sampling. Subsample. Analyte A. Result A. QC. LIMS. Total Sample results. LIMS. Subsample. Analyte B. Result B. QC. Sample. Other sample info and invoice data. Subsample. Analyte C. Result C. QC. Subsample. Analyte D. Result D.
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Flowchart for the Laboratory Sampling Subsample Analyte A Result A QC LIMS Total Sample results LIMS Subsample Analyte B Result B QC Sample Other sample info and invoice data Subsample Analyte C Result C QC Subsample Analyte D Result D QC Logistic Analyte D Result D QC Subsample Result Y Final approval & signiture Sub- suplying lab Analytical report Invoice Analyte Y Customer
LIMS - VAXLIMS • Laboratory Information Management System • Information on sampling sites • Information on customers (orders) • Information on individual analytic programmes • Gives unique ID number to samples • Samples and subsamples are barcoded • Barcodes gives information to instruments and instruments returns results to VAXLIMS • Sample information etc. can be accessed from other ROVESTA departments (Holbæk, Næstved) • VAXLIMS produces final analytical reports and data for invoices
Analytical selection • Waste water: • pH • Suspended solids • Biochemical and chemical oxygen demand (BOD & COD) • Nitrite, nitrate, ammonium, kjeldahl-N and total nitrogen • Ortho phosphate and total phosphorus • Chloride • Sulfate
Analytical selection • Fresh- and seawater: • Suspended solids • Biochemical oxygen demand (BOD) • Nitrite, nitrate, ammonium and total nitrogen • Ortho phosphate and total phosphorus • Silicate • Chlorophyll
Analytical selection • Drinking water: • pH, conductivity, oxygen • Total solids, color, turbidity • Bicarbonate • Nitrite, nitrate, ammonium • Total phosphorus • Chloride, sulfate, fluoride • Hydrogen sulfide
Analytical selection • Sludge: • Total solids • Volatile solids • Total nitrogen • Nitrite+nitrate, ammonium, ortho-P (special)
Quality System – DS/EN ISO 17025 • Part 1: Management requirements • Organization • Quality System • Document control • Review of requests, tenders and contracts • Subcontracting of tests and calibrations • Purchasing services and supplies • Service to clients - complaints • Control of nonconforming tests • Corrective and preventive action • Internal audits • Management reviews
Quality System – DS/EN ISO 17025 • Part 2: Technical requirements • General • Personnel • Accommodation and environmental conditions • Test methods and method validation • Equipment • Measurement tracebility • Sampling • Handling of test items • Assuring the quality of test results • Reporting the results