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WellLock ® Resin System

WellLock ® Resin System. WellLock ® Resin System – Applications. Remediation Low viscosity Penetrates Micron-sizes pores Resists Gas Channeling Secondary Annular Barrier Increased elasiticity High-pressure seal Compressive Strength Plug to Abandon Tolerates impurities

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WellLock ® Resin System

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  1. WellLock®Resin System

  2. WellLock® Resin System – Applications • Remediation • Low viscosity • Penetrates Micron-sizes pores • Resists Gas Channeling • Secondary Annular Barrier • Increased elasiticity • High-pressure seal • Compressive Strength • Plug to Abandon • Tolerates impurities • Withstand high-pressure differentials • Injection (Disposal) Wells • Fluid compatibility (including water) • Chemical and corrosion resistant Stress: 4500 psi Strain: 50%

  3. WellLock® Resin System • High pressure seal (1,000 psi/ft) • Chemically resistant (acid/CO2) • Withstands contamination (overcomes inefficient mud displacement) • Increased elasticity (up to 20%) • Compressive strength (5 to 15 kpsi) • No yield point as a liquid • Drillable

  4. WellLock®Resin System A cross-linking reaction between an amine hardener and epoxides, resulting in a cured three-dimensional infinite polymer network. • Control of reaction rate achieved through chemistry • Adjust accelerator concentration to achieve desired pumptime and compressive strength development • longer working times lead to longer compressive strength development

  5. WellLock®Resin System A cross-linking reaction between an amine hardener and epoxides, resulting in a cured three-dimensional infinite polymer network. • Control of reaction rate achieved through chemistry • Adjust accelerator concentration to achieve desired pumptime and compressive strength development • longer working times lead to longer compressive strength development

  6. WellLock®Resin System HPHT Thickening Time Chart at 175°F

  7. WellLock®Resin System – Rheological Behavior Herschel-Bulkley/ Bingham Plastic Newtonian

  8. WellLock®Resin System When tested in an environmental chamber at a downhole temperature of 162°F (72°C), WellLock resin achieved 12,500 psi and remained highly elastic. ®

  9. WellLock®Resin SystemAnnular Hydraulic Seal Test • System constructed from 1 ft pipe nipple with steel bar welded into center • Test fluid chamber and test cell can be immersed in a water bath for temperature control • WellLock®resin system completely prevented flow at 1,000 psi fluid pressure

  10. WellLock®Resin System • Complements cement • High pressure seal • Chemically resistant • Withstands impurities • Increased ductility • Compressive strength Resin Film Cement Formation Casing

  11. WellLock®Resin System Lead resin slurry deposits film on formation and casing resulting in dramatic shear bond improvements.

  12. WellLock®Resin System Mud Contaminated Compressive Strength • 15.2 lb/gal WellLock®Resin • 15.0 lb/gal synthetic based mud

  13. WellLock® Resin – Properties Comparison Water WellLock Resin

  14. WellLock®Resin SystemField Blending and Placement • Job type • Secondary barrier • Remediation • Planning • Current wellbore conditions • Placement time • Fluid train • Compatibility • Spacers • Placement • Batch mix components • HT-400™pump • Coiled tubing • Drill string • Tubing

  15. WellLock®Resin System Remedial work where particle-laden fluids are unable to penetrate problem areas. • Tight Casing Leaks • Gravel Packs After: Resin penetrates for impermeable seal Before: water breakthrough in gravel pack

  16. Offshore Challenge Produced water interfering with production and creating disposal costs Potential for on-going casing erosion due to gravel-pack flow back Suggested Solution Squeeze job WellLock®Resin (6 bbl) Anticipated Result Resin placed at the breakthrough area Water cut eliminated WellLock®Resin System – ApplicationRemediation

  17. WellLock®Resin System Secondary annular barrier to help maintain long term wellbore integrity during aggressive completion operations.

  18. Shale-Play Challenge High-concentration of fracture placement Increased regulatory focus on fracture stimulation Environmental sensitivities regarding water table Suggested Solution – Three-stage cementing operation inclusive of secondary barrier Lead cement (50 to 100 bbl) WellLock®Resin (20 bbl) Tail cement (50 to 100 bbl of LifeCem™ Cement) Anticipated Result Casing-to-casing barrier Corrosion resistant, gas-impermeable seal Environmental sustainability WellLock®Resin System – Application Secondary Barrier

  19. WellLock®Resin System Plug and Abandonment • Withstands impurities during placement • High bond strength • Withstands extremely high pressure differentials

  20. WellLock®Resin System – From the Field • Challenge • Multiple conventional P&A attempts failed (continuous bubbles rising to the surface due to small leak in the annulus between the 30-in.drive pipe and the 20-in.conductor pipe) • Costs accruing as rig is unable to move off of well until tests proved successful P&A • Solution: WellLock®Resin / 2 different operations • 10 bbl squeeze application • 50-ft resin plug set in the 13.3/8 casing • Result • Successful bubble test (bubbles ceased) allowing plug operation to proceed • Successful Plug operation allowed casing to be cut • Well permanently abandon and rig moved to next well

  21. WellLock®Resin System – From the Field • Challenge: Salt (brine) Cavern • Micro-annulus on the back side of the production casing with leak off rate in the <100 bbls/year • Unable to pass MIT • Solution: WellLock®Resin • Bradenhead squeeze fromthe top of the annulus • Extremely tight microannulusaccepted only 0.6 bblof resin via surface valve • Results • Rain during operations did not negatively affect resin (unlike conventional epoxies) • Passed an MIT gradient of .86-.87 ppg • Expense of running / cementing an additional pipe string avoided

  22. WellLock®Resin System – From the Field • Challenge: Marcellus Shale Annular Pressure Buildup • Having cemented the intermediate casing, the well registered gas flowing to surface • Operator chose to suspend drilling next stage until successfully remediating for APB • Solution: WellLock®Resin (solids free / neat resin) • Perforated and set packer at 933 ft. • Squeeze application fluid train: water (20 bbl)  WellLock resin (10 bbl)  FineCem™ cement (6 bbl) • Results – First ever application involving displacement of resin by cement • Formation accepted all 10 bbl of WellLock Resin • Pumping pressure drop observed when resin reach the perforations • Annular gas flow dropped throughout operations • Drill-out began 60 hours after the operation – zero gas flow detected

  23. WellLock®Resin System – From the Field • Challenge: Shale - Annular Pressure Buildup on the intermediate casing. • Solution: Three-stage WellLock®Resin operation • Set drillable bridge plug, perforate, set retainer, squeeze 10 bblresin into perfsfollowed by10 bblFineCem™ cement • Perforate higher, set retainer, squeeze 10 bblresin into perfs followed by 20 bblFineCem cement into perfs • Perforate higher, set retainer, squeeze 10 bblresin into perfs followed by 20 bblFineCem cement • Results • Formation accepted all resin, leaving planned amount of FineCemcement in casing at each stage – easily drilled out • Gas flow on the backside eliminated

  24. WellLock®Resin System – From the Field • Challenge: Shale / Continental Europe • Drilling suspended due to damaged inflatable packer in 4½-in. and 9-5/8-in. annulus • Unable to achieve pressures needed for fracture stimulation operations to complete the well and bring it onto production • Solution: WellLock®Resin • Using coiled tubing, place 1.5 cubic meters of WellLock above drillable bridge plug previously set in 4½-in. casing below leak • Open 9-5/8-in. annulus to circulate 1 cubic meter of resin through leak into annulus leaving 0.5 cubic meters in casing • Allow to cure • Results • Resin withstood pressure test of 7500 psi and was successfully milled out • Drilling operations resumed

  25. WellLock®Resin System: Halliburton Firsts • First time to successfully displace a resin with a cement • Partial immiscibility allows resin to stay isolated from the slurry and develop high strength • Resin system remains pure and uncontaminated, forming a gas-impermeable infinite polymer network • Gas flow completely shut down

  26. WellLock®Resin System – Summary • As a product: • Enhances the long term integrity of the well • Unique mechanical properties and chemical resistance • Rheological profile leads to deep penetration into tight crevices • As a service: • Engineering and planning to customize design for maximum usage and effectiveness of material • Laboratory support from Houston Technology Center • As a solution: • Addresses gas migration • Non-porous secondary barrier

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