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Process. Epoxy adhesion to control the sensing area over night. Wash by DI water. Dry by N 2 (g). Dip 3ml 1N NaOH for 10min. Dry by N 2 (g). Dip 3ml prepared solution for 50min. at 37-38℃. Dip 3ml 1N HCl for 10min. Wash by DI water. Dry by N 2 (g). Dry by N 2 (g). Scan CV (bare Au).
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Process Epoxy adhesion to control the sensing area over night Wash by DI water Dry by N2(g) Dip 3ml 1N NaOH for 10min. Dry by N2(g) Dip 3ml prepared solution for 50min. at 37-38℃ Dip 3ml 1N HCl for 10min. Wash by DI water Dry by N2(g) Dry by N2(g) Scan CV (bare Au) Scan CV (adsorbed)
Fig 1. The cyclic voltammetry of Au electrode WE: Au-Cr coated on silicone wafer by e-beam, 0.125 cm2, RE: Ag/AgCl(0.5MKCl), CE: Pt, Electrolyte: 0.5 M KCl +20 mM K4Fe(CN)6+20 mM K3Fe(CN)6), Scan range: -0.20~0.60 V, Scan rate: 0.05 V/sec
Table Ⅶ : The table of peak current *8ppm albumin /0.5MKCl/PH=3.51(1N HCl) *adsorb temperature 37-38℃
Fig 2. The renewing test of Au electrode WE: Adsorbed Au-Cr coated on silicone wafer by e-beam, 0.125 cm2, RE: SCE, CE: Pt, Electrolyte: 0.2 M H2SO4, Scan range: -0.20~0.60 V, Scan rate: 0.05 V/sec