1 / 11

Liquid-Liquid Extraction

Liquid-Liquid Extraction. Group 5 Alex Guerrero Andrew Duffy Bernard Hsu Daniyal Qamar Jeff Tyska Ryan Kosak Tomi Damo. ChE 382 2/10/2011. Introduction. In this laboratory, Acetic Acid in Oil will be extracted by water. Oil = Raffinate Water = Extract Counter-Current Flow.

sitara
Download Presentation

Liquid-Liquid Extraction

An Image/Link below is provided (as is) to download presentation Download Policy: Content on the Website is provided to you AS IS for your information and personal use and may not be sold / licensed / shared on other websites without getting consent from its author. Content is provided to you AS IS for your information and personal use only. Download presentation by click this link. While downloading, if for some reason you are not able to download a presentation, the publisher may have deleted the file from their server. During download, if you can't get a presentation, the file might be deleted by the publisher.

E N D

Presentation Transcript

  1. Liquid-Liquid Extraction • Group 5 • Alex Guerrero • Andrew Duffy • Bernard Hsu • DaniyalQamar • Jeff Tyska • Ryan Kosak • TomiDamo ChE 382 2/10/2011

  2. Introduction • In this laboratory, Acetic Acid in Oil will be extracted by water. • Oil = Raffinate • Water = Extract • Counter-Current Flow

  3. Purpose • The purpose of this experiment is to operate the three-stage mixer/settler system to extract Acetic Acid from White Oil using water as a solvent, while we investigate the effect of the speed of mixing on the extraction efficiency. • The efficiencies calculated will be the Murphree Efficiencies.

  4. Theory • Liquid-Liquid Extraction works because of differences in the solubility of the solute in the extract and raffinate. • Polar and Non-Polar Compounds, “like mixes with like.” • Acetic Acid dissolves more readily in water than oil • Water and oil do not mix • Acetic Acid is removed from oil due to solubility with water.

  5. Theory • = composition of extract phase equilibrium with raffinate phase leaving the (S+1)th stage. • Ys = real composition of the extract phase leaving the (S)th stage • Y(s+1) = real composition of the extract phase leaving the (S+1)th stage

  6. Theory • = composition of the raffinate phase in equilibrium with extract phase leaving the (s+1)th phase. • Xs = real composition of the raffinate leaving the (S)th stage • x (s+1) = real composition of the raffinate leaving the (s+1)th stage

  7. Theory • = theoretical number of stages required • = actual number of stages used • %Removal = (x(in) – x(out))*100/(x(in)) • %Removal in nth stage = (x(n)-x(n+1))*100/(x(n))

  8. Apparatus

  9. Materials

  10. Safety • Oil/water Spills • Slippery Conditions • Glacial Acetic Acid • Corrosive • Vapors • Electrical Equipment

  11. References • Wankat, P. C., (2007). Separation Process Engineering (2nd ed.).New York: Prentice Hall • Hyfoma. Extraction. http://www.hyfoma.com/en/content/processing-technology/separation-techniques/extraction/ • "MatWeb - The Online Materials Information Resource." Online Materials Information Resource - MatWeb. Web. 23 Jan. 2011. <http://www.matweb.com/search/datasheet.aspx?matguid=ab1fc45899a5464a8655448211643b1d&ckck=1>

More Related