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Introduction to Analytical Chemistry. Dr Carl Hall X1/12 c.e.hall@hud.ac.uk. SFC1004 Analytical Science 1. Module Outline. 24 Lectures Tuesdays 11.15 - 12.15 Autumn Term - Carl Hall Spring Term - Richard Southam 24 Tutorials Tuesdays 12.15 - 1.15 6 four hour labs
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Introduction to Analytical Chemistry Dr Carl Hall X1/12 c.e.hall@hud.ac.uk SFC1004 Analytical Science 1
Module Outline • 24 Lectures • Tuesdays 11.15 - 12.15 • Autumn Term - Carl Hall • Spring Term - Richard Southam • 24 Tutorials • Tuesdays 12.15 - 1.15 • 6 four hour labs • Last six weeks of Spring term
Module Outline • Lectures • The PowerPoint lecture material is only the outline of the course YOU NEED TO MAKE YOUR OWN NOTES AS WELL! • Handouts will be available at beginning of lecture. • The lecture material is also available from the Universities Blackboard website at http://vitual.hud.ac.uk. http://www.hud.ac.uk http://icilda.hud.ac.uk/?bbatt=Y
Assessment Profile • Continuous Assessment - 35% • Tutorials in Autumn term - 10 minute MCQ tests based on selected tutorial questions. • Weekly feedback for students • Identifies strengths and weaknesses • Ensures that tutorial work is completed • Removes the need for additional assessments • Practicals - 25% • Exam - 40% • 2 x 1 hour tests in weeks 16 and 31
Outline Syllabus • Quantitative Analysis • Types of method • Units • Data Handling • Significant figures • Origin of errors • Estimation of uncertainty • Accuracy and Precision • Basic Statistics • Data presentation
Outline Syllabus • Titrimetric analysis • Gravimetric analysis • Colorimetric analysis • Spectroscopic Analysis • Infra-red - ir • UV visible
References • Quantitative Chemical Analysis • Daniel Harris - 6th Edition - 2002 • Supporting material available on website • Exploring Chemical Analysis • Daniel Harris - 2nd Edition - 2001 • Analytical Chemistry - An Introduction • Skoog, West, Holler and Crouch - 7th Edition - 2000 • Quantitative Chemical Analysis • Vogel - 6th Edition
References • Introduction to Spectroscopy • Pavia, Lampman and Kriz - 2nd Edition - 1996 • The Molecular World - Separation, Purification and Identification • Lesley Smart - 2002 • Spectroscopic Methods in Organic Chemistry • Dudley Williams and Ian Fleming - 5th Edition -1995