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PERVİN ARIKAN Gazi University - ANKARA

TARLA Tesisi İstasyonları ve AR-GE Potansiyeli. PERVİN ARIKAN Gazi University - ANKARA. 0 7-09 . 09. 2013, Türk Fizik Derneği 5. Uluslararası Katılımlı Parçacık Hızlandırıcıları ve Uygulamaları Kongresi (UPHUK-5). Outline. List of Staff Planning of experimental stations

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PERVİN ARIKAN Gazi University - ANKARA

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  1. TARLA Tesisi İstasyonları ve AR-GE Potansiyeli PERVİN ARIKAN Gazi University - ANKARA 07-09.09.2013, Türk Fizik Derneği 5. Uluslararası Katılımlı Parçacık Hızlandırıcıları ve Uygulamaları Kongresi (UPHUK-5)

  2. Outline • List of Staff • Planning of experimental stations • Techniques and application fields • Working groups • Infrastructure of Labs. • User potential • CALIPSO and ESUO • HORIZON 2020 • TARLA II Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  3. TARLA IR FEL Laboratories • are charged with the responsibility to supply state-of-the-art radiation in broad region to a diverse user community. • Scientific opportunities in physics,chemistry, biology and medicine are investigated to foster new research areas in Turkey and region Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  4. TARLA-IR FEL Exp.Stations and User Potential - Working Group • Dr. Pervin Arıkan ( Gazi University) Coordinator • Dr.İlhan Tapan (Uludağ University ) ( photon diagnostics ) • Dr.Atilla Aydın ( Bilkent University ) ( IR Spect.material charact. ) • Dr.Ayşe Hiçsönmez ( Ankara University) ( medicial appl. ) • Dr.Feride Severcan ( METU) (bio-micro Spectroscopy ) • Dr.Hakan Altan ( METU ) ( ultrafast photonics) • Dr.Okan Esentürk ( METU) ( ultrafast photonics) • Dr. Ömer İlday ( Bilkent University ) ( material processing ) • Dr.Ergün Kasap ( Gazi University) ( optical beamline transport ) • Müge Tural Gündoğan ( Ph.D Student - Ankara University) (M.Sc. IRFEL Labs.) • Ayşegül Uşun ( M.Sc. – Gazi University) ( pump-probe) • Elif Tatoğlu ( M.Sc. - Gazi University) ( IR Spect. ) • Selin Erdoğan ( M.Sc. - Gazi University) ( SFG) • Emre Erbay ( Ph.D student- ÖİB University) ( M.Sc. optical beamline transport ) • Begüm Tekiner ( M.Sc. - Ankara University) (optical beamline transport ) • Kamile Tekfidan (M.Sc. - Gazi University) (optical beamline transport ) • Ersin Çiçek (M.Sc. - Gazi University) ( photon diagnostics ) • İdil Arslan ( M.Sc - Ankara University) ) ( photon diagnostics ) Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  5. TARLA IR FEL & Brems facility Cooling & Generator Rooms Analysis, Control, Atelier Rooms ExperimentHalls Accelerator and FEL Production Area Accelerator and FEL Production Area Klystron, Electronics Room Bremsstrahlung Experiment Area 5 Pervin ARIKAN | Gazi University

  6. The obtained laser ( 3 -250 μm) will be delivered to experimental stations ( MIR and FIR region ) • 1. Photon diagnostıcs lab. 2. Infrared spectroscopy laboratory ( IR Lab.) material characterization 3.Pump-probe /sum frequncy generation laboratory( PPT/SFG) • Other laboratories will be prioritized with respect to the needs and requirements of the expected proposals of the researchers in the areas outlines previously. • It is imperative that the photon beam is well prepared for transport and well diagnosed before experiments can be conducted these laboratories Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  7. IRFEL Experimental Stations of TARLA Facility Coordinator :Dr.Pervin Arıkan ( Gazi Univ.) • Photon Diagnostics ( Lab 1) Dr. İlhan Tapan (Uludağ Univ.) • Ultrafast Photonics Applications ( Lab 2) Dr.Okan Esentürk and Dr. Hakan Altan ( METU) • IR Spect. (Material Charact.) ( Lab 3) Dr. Atilla Aydınlı (Bilkent Univ. ) Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  8. Main application field of IR FEL • Photon Science • Material Science • Semiconductors • Biotechnological and medical research • Non-linear Optics • Nanotechnology • Photo-Chemistry Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  9. Experimental techniques 1 - Sum Frequency Generation 2 - Photon Echo Experiment 3 - Photoacustic Spectroscopy 4 - Pump-Probe Techniques 5 - IR-MALDI (IR matrix assisted laser desorption/ionization ) 6 - IR-MAPLE ( IR matrix assisted pulsed laser evaporation ) 7 - IR-REMPI (IR resonance enhanced multiphoton ionization) 8 - Near Field Microscopy Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  10. Photon Diagnostics Lab. * Ersin Çiçek, SEL için Foton Diyagnostiği’nin Teknik tasarımı, 08.09.2013, UPHUK-V Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  11. Needs of the Industrial and Scientific Community in Turkey • Characterization of electrical properties of solar cells • Characterization of the crystal or amorphous materials used in the production of thin-film solar cells • Understanding the effect of thermal stress on material longevity • Measurement on deposited films or coatings using ultrafast techniques • Dynamical characterization of detector response in the infrared and visible regions • Characterization and calibration of eye-safe CCD and/or CMOS detectors • Characterization of power and output characteristics of Quantum Cascade Lasers (QCL) • Time-domain characterization of point-like bolometer detectors or micro-bolometer arrays • Understanding working principles of dynamical catalysis mechanisms in various reactions • Characterizing polymer surfaces that can be utilized in biosensors, batteries, and other electronic devices. 12

  12. IRFEL material characterization (Lab layout ) u Soğutma suyu N2 Raman kryostat ukop FTIR Krayo NSOM fs lazer Vak Veri toplama Y. Parça,sarf, stok Güç Basınçlı hava Örnek hazırlama Vakum

  13. Time Resolved Vibrational Spectroscopy of Chemical Reactions • One narrowband ultrafast IR laser pulse excites vibrational modes in a molecule and is followed by a second broadband infrared pulse, which gives two independent frequency axes and allows the collection of 2D-IR spectra. • Spectra provide direct information on vibrational anharmonicities, energy transfer processes, and molecular structure. http://www.cchem.berkeley.edu/cbhgrp/

  14. Time Resolved Vibrational Spectroscopy of materials • Examine the structures and charge carrier dynamics of photovoltaic materials.  • Use • Two-dimensional infrared (2D IR), • Polarization resolved dispersed IR pump-probe, • Visible pump–IR probe (vis-IR) spectroscopy.  • Study solar energy conversion including:  • Excitation transport, • Free carrier formation • Carrier diffusion   • Bimolecular charge recombination and charge trapping.

  15. Spectroscopy of the Solid State • Carrier dynamics: • Quantum wells, superlattices, and quantum dots (e.g. • inter- and intra-subband/miniband relaxation, Bloch • oscillations) • Infrared and THz properties: • Electrically driven quantum structures (Bloch oscillators • and quantumcascade lasers) • Resonant coherent effects: • High-intensity laser pulses closely resonant with the • intersubband energy can induce coherent phenomena • such as dressed states and Rabi oscillations • Electron dynamics: • Ultrashort IR pulses with controlled phases.

  16. 3.5m SFG ~6m Pump/ Probe • Ultrafast Photonics Applications Laboratory Lab Layout >1mJ, 1kHz synchronized, sub-100fs ultrafast amplified laser source at 800nm center wavelength mJ pulse energies for a wavelength range of 200-11000nm Main Experiments will be centered around pump/probe measurements and sum-frequency generation measurements. All experiments are planned to start pre-FEL beam Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  17. Pump-Probe Method • Pump-probe method enables to follow in real time vibrational motions coupled to electronic transitions. The sample is excited by one pulse train (pump) and the changes it induces in the sample are probed by the second pulse train (probe), which is suitably delayed with respect to the pump.Changes in the order of picosecond can be observed with this method.

  18. Pump/Probe Experiment • With jitters less than 1ps, many dynamical pheonomena in fast materials can be measured. • Once the beam is in the lab there will be two permanent home-built systems, one of which is the pump-probe system (the other SFG) • This system will allow the user to utilize both the short wavelength ultrafast laser system (200-11000nm) or the FEL system (2-250mm) either separately, or at the same time • Using mechanical delay stages, by changing the delay between the pump and probe beams, and utilizing appropriate detectors that can measure the change in intensity of the probe beam (ie. IR diode detectors, bolometers, MCT detectors, etc.) Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  19. Sum Frequency Generation (SFG) Spectroscopy Sum Frequency Generation (SFG) is a nonlinear optical technique used to study the details of molecular structure and dynamics at surfaces and interfaces. SFG has advantages in its ability to be monolayer surface sensitive, ability to be performed in situ (for example aqueous surfaces and in gases), and not causing much damage to the sample surface. This spectroscopy method utilizes SFG, where two light beams mix at a surface and generate an output beam with a frequency equal to the sum of the two input frequencies. From the experiment setup and the output beam, one can deduce the composition, orientation distributions, and some structural information of molecules on a surface.

  20. SFG = VIS +IR IR Vapor VIS Interface c(2) = 0 in isotropic media c(2) 0 in interface Liquid { c(2) (x,y,z) = -c(2) (-x,-y,-z) • Sum Frequency Generation (SFG) Experiment • Advantages • Surface specific • Molecularly specific • Low conc. sensitivity • Orientation & conformation • In situ and non-destructive Interface sums the incoming frequencies P = P(0) + P(1) + P(2) … P(2) = c(2) E(w1) E(w2) I(w3) a| P(2) | 2a |c(2)|2 I(w1) I(w2) Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  21. Planned and needed services in the Labs • Air-condition • UPS • Liquid helium • Water free nitrogen • Oil free air pressure • Cooling water • Liquid nitrogen • Temperature control • Dust ( particle) control • Humidity control • 220-400 Voltage • 40 kW per room • LAN Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  22. USER POTENTIAL We identified areas of interest and contacted spesific researchers since 2009 . Few areas of interest • Conventional Laser ve IR FEL • Non-linear optics • Pump-probe Techniques • Sum frequency generation • FTIR , Raman Spect. • Optics and signal process • Terahertz Spect. • Nanotechnology • Material Science • Semi-conductors • IR Imaging • Laser ablation • Nanomedicine Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  23. First User Meeting 2009 Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  24. Second User Meeting -2010 Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  25. Main laser and optics research center in universities • Kocaeli University (LATARUM) İzmit • METU (Material science and THz lab.) Ankara • Ankara University(Nonlinear optics Lab.) Ankara • Bilkent University( Advanced technology research center + UNAM National nanotechnology research center)Ankara • Koç University(LASER Lab.)İstanbul • UME (Optical Lab.) İzmit • SABANCI University(Optical Lab.)İstanbul • İzmir Advanced Technology Institute ( chemistry) Ankara Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  26. USERS in TURKEY Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  27. INTERNATIONAL RELATIONS • EU SEVENTH FRAMEWORK PROGRAMME • Combination of Collaborative Projects And Coordination and Support Actions for Integrating Activities • INFRA-2012-1-1.23:Synchrotron radiation sources and Free Electron Lasers Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  28. EU-FP-7 INTERNATIONAL RELATIONS Title : Coordinated Access to Light sources to Promote Standards and Optimization Budget : 10 M Euro Duration : 36 months ( June 2012 – May 2015) Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  29. Project management of CALIPSO • Dr. Michele Bertolo, • Head of Sponsored Research Office at Sincrotrone Trieste S.C.p.A.(Elettra) ITALY • Dr. Cecilia Blasetti ,(Managing Team ) Elettra • “wayforlight”portal • http://www.wayforlight.eu • www.esuo.org Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  30. Objectivesof CALIPSO ** CALIPSO coordinates the European synchrotrons and FELs towards a fully integrated network. ** The consortium is characterized by common objectives,harmonized decisions, strong communication,transnational open access based on excellence and joint development of new instruments. Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  31. The20 consortium members of CALIPSO • ALBA • AU(ISA) • CLIO(CNRS) • DESY • Diamond • Elettra • EMBL • ESRF • BESSY(HZB) • FELBE(HZDR) • ANKA(KIT) • INFN • MAXIV • PSI-SLS • FELIX(RU) • SOLARIS • SOLEIL • STFC • TAC • XFEL Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  32. Members of CALIPSO Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  33. CALIPSO ACTIVITIES **Networking Activities/NAs Wayforlight (ESUO) and HERCULE School **Transnational Access Activities/TAAs 14 Accelerator Facility-Users Project ** Joint Research Activities/JRAs • FELSEED , HIZPAD2 , NanoFOX+ Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  34. European Accl. Users Organization CALIPSO-ESUO • TAC-TARLA is member of ESUO (CALIPSO - TAAs ) • 14 Accelerator Facility-Users Project • National delegate system ( Prof.Pervin Arikan) • ESUO 5 Meeting 19-20 Sep. 2013 PSI Switzerland Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  35. HORIZON 2020 • Dr. Josef FELDHAUS Head of FLASH operation group – DESY Photon Science • Chair of the Collaboration of European FEL and SPS Facilities (SPS=accelerator based short-pulse sources). • With the presentproposal we suggest to consider the emerging and fast developing field of free electron lasers as a separate topic for the EU programHorizon 2020.(Horizon 2020, the EU's Research & Innovation funding programme for 2014-2020 ) * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * • Since CALIPSO also includes several IR FELs and since there will be a separate FEL topic for an I3 under HORIZON2020 (following the EC consultation last fall which you certainly remember), • We would like to invite your institute also to join our activities and become member of the Collaboration. The operating facilities CLIO, FELBE and FELIX have already indicated their interest and are ready to sign the MoU. Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  36. ROAD MAP • As a first step , planning of 3 experimental stations • TDR and construction • Practical experience of users ( CALIPSO TAA ) • Teaching and training of junior staff • Determine user profile of Turkey • CALIPSO • ESUO • HORIZON 2020 • LSUM2013 ( 4-6 October 2013 , HTE-Ankara Univ.) • TARLA II Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  37. TARLA II PROJECT • Aim of TARLA II Project: • To get additional budget and time to complete the TARLA facility including • 5 (IR FEL) and 1 (Brems.) experimental stations. • Planned project period: (5 years) • Proposed project budget: 25 MEuro (~ 60 MTL) • Collaboration: • Ankara, Gazi, S. Demirel, İstanbul, Bilkent, METU, Uludağ • Universities

  38. TARLA II PROJECT • Project Team: • Ankara U.: • Ö. Yavaş, A. Hiçsönmez, A. Aksoy, Z. Nergiz, Ç. Kaya, Ö. Karslı, B. Koç, E. Kazancı, M. Aydar,.... • Gazi U.: • P. Arıkan, E. Çiçek,.... • S. Demirel U.: • G. Yeğin, E. Kürkçüoğlu, A.G. Kalaycı, M. Şekerci, ..... • İstanbul U. • S. Özkorucuklu, • METU: • F. Severcan, H. Altan, O. Esentürk,.... • Bilkent U.: • A. Aydınlı, Ö. İlday,.... • Uludag U.: • İ. Tapan, E. Pilçer, F. Kocak, ... • + ~20 Engineers, Technicians, MSc and PhD Students

  39. Layout FEL BEAM • A: Diagnostic • 6 x 6.7 x 4.2 m (w x l x h) • B: Ultrafast • 6 x 10 x 4.2 m • C: IR • 6 x 7.2 x 4.2 m • D: Material Processing • 6 x 7.5 x 4.2 m • E: Biology • 6 x 7.5 x 4.2 m 40

  40. Designated Labs at TARLA Facility Diagnostic Lab FEL I & II Ultrafast Photonics Applications Laboratory Bio-Micro Spectroscopy Lab FEL BEAM IR Spectroscopy Lab Materials Processing Lab • There are 5 laboratories in total. There is overlap among experiments that will be conducted in these laboratories. 41 Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  41. Bio-Micro Spectroscopy Laboratory Measurements will be centered around similar work done by project leader at Brookhaven National Laboratories utilizing Synchrotron-FTIR techniques. These techniques will be adapted to the TARLA-FEL beam. Capabilites will include both spectroscopy and imaging of biological specimens. Coupled with collaboration from the medical school of Ankara University the laboratory is expected to become a premier center for biological reserach. Experiments are planned for pre-FEL start 42

  42. Bio-Micro Spectroscopy Laboratory 43 In this laboratory, together with multivariate statistical analytical methods, many different topics, that realte to important areas for medical applications will be investigated. Some are: Identification of disease induced alterations in dynamic, structure and content of macromolecules in the level of tissue, cell, organelle and biological fluid, Determination of biomarkers which can be used in the early diagnosis of diseases,Following of the disease progression, examination of the treatment strategies and the efficacy of treatment methods Several radiobiological investigations including the determination of the radiation dose and the effects of radiation, Determination of postmortem interval, fingerprint, presence of illicit drugs in biological samples, Examination of the effects of environmental pollutants on living organisms such as fish, plant, water flea etc. Investigation of the possible usage of organisms to find out biomarkers in characterization of the environmental pollutants, Identification of food and beverage quality in Food Industry, Identification of bacteria species in Microbiology, Diagnosis and characterization of disease and stress factors in plants

  43. Material Processes Lab. 44 With increased laser power and beam qualitymore and more application fields were developed and meanwhile laser processes can be foundin nearly all production areas and branches .

  44. Prof.Dr. Arif DEMİR ve ekibinin çalışmaları 1- Laser Technologies Research and Application Center - LATARUM 2- Fundamental laser parameters in material processing (pulse duration, wavelength, pulse energy, repetation rate) 3- Millisecond laser material processing welding (titanyum, magnesium ) cladding, cutting (stainless steel) drilling (ceramic) 4- Nanosecond laser material processing drilling ceramic, LIBS, thin film coating 5-Femtosecond laser metarial processing hydrofobic and hydrofilic surfaces nanoparticle production 45

  45. Conclusions • We intensively wish to obtain the good results for the first facility which will be used for TAC’s further steps… • Turkey and the region has good potential to use such a facility and completion of TAC will give impuls and oppurtunities to researchers to use new and modern tools Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  46. Thank you for your attention… Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  47. Physical requirements • Area = 42 m2 • Dimensions = 6x7 m2 • Height = 3.5 m • Floor = zemin • Environmentalrequirements: • Temperature : 21.0 ± 1.0 oC • Humidity : % 45 ± %10. • Services required: • Pressurizedcleanroom (class 10000) • Coolingwater (> 7 bar) • Pressurizeddryair (> 3 bar) • UPS (min 5kVA ) • 220V ve 380V / 50Hz • Gasandliquidnitrogenandliquidhelium. Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  48. Laboratories • Ultrafast Photonics Applications Laboratory • Lab Coordinators : Hakan Altan (Physics METU), Okan Esentürk (Chemistry METU) • IR Spectroscopy Laboratory • Lab Coordinator: Atilla Aydınlı (Physics Bilkent) • Biological Micro Spectroscopy Laboratory • Lab Coordinator: Feride Severcan (Biology METU) • Material Processing Laboratory • Lab Coordinator: F. Ömer İlday (Physics Bilkent) METU and Bilkent University are new team members Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

  49. Demet Sıkıştırıcı • Schematic View of TAC IR-FEL & Brems. Facility Enjektör 250 keV LINAK-1 5-20 MeV LINAK-2 8-40 MeV Lazer 3-250 µm SEL Üretimi * Suat Özkorucuklu, THM TARLA Tesisi, 09.09.2013, UPHUK-V 50 Pervin ARIKAN | Gazi University, 07-09.09.2013 UPHUK-5

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