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APS8_34

APS8_34. Al90Tb10 RTO-2-9 MJK. Heated at 10C/min 6 s per scan Did a 21 point data smooth of T data T-t data file: APS8_34_heating_all_smooth21 Combined the 2 GE1 data sets as a first look Good data for c1_00311 Starts at 455s Crystallization begins at 1403 s Good data for c2_00312

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APS8_34

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  1. APS8_34 Al90Tb10RTO-2-9MJK

  2. Heated at 10C/min • 6 s per scan • Did a 21 point data smooth of T data • T-t data file: APS8_34_heating_all_smooth21 • Combined the 2 GE1 data sets as a first look • Good data for c1_00311 • Starts at 455s • Crystallization begins at 1403 s • Good data for c2_00312 • Starts at 1907 s • Cooling at 3251 s

  3. Time sequence • Initial crystallization • Initial ~ 229°C • Final ~ 237°C • 4 crystallization events

  4. Initial crystallization • Subtract scan 150 • Small amount of fcc Al appears first

  5. Cry fraction only • Convert to two theta and then output in gsas format • Scan 1 is at time 1361, 220C

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