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Learn about the informative power of Fourier Transform Infrared (FT-IR) spectroscopy, a non-destructive and rapid analysis method. This technique offers direct sample analysis, minimal sample preparation, and database matching for unknown compound identification. By utilizing chemical functional group strengths or spectral characteristics, FT-IR enables quantitative analysis without chemical reagents, environmental pollution, or safety hazards.
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Why used FTIR 非破壞性分析 , 操作簡單 , 分析快速 樣品直接分析 , 幾乎勿需前處理 配合資料庫搜尋,可作未知物分析 可利用化學官能基強度或光譜特性變化 , 來做定量分析 無需化學試劑 , 無環境污染問題 , 安全無污染
Introduction: The Electromagnetic Spectrum IncreasingWavelength 50,000 12,820 4000 400 cm-1 Gamma X-ray UV NIR IR FIR Micro Radio 200 380 780 2500 25 000 nm Increasing Energy K-shell electrons Outer-shell electrons Molecular vibrations Molecular Rotation
Infrared (IR) Spectroscopy…. O H H -C-H 2850-2960 cm-1 -C=O 1640-1750 cm-1 =C-H 3020-3100 cm-1 -C-O 1050-1150 cm-1 -C=C- 1650-1670 cm-1 -O-H 3400-3640 cm-1 -C-Cl 600-800 cm-1 -N-H 3310-3500 cm-1 -C-Br 500-600 cm-1 IR Spectroscopy measures the radiation absorbed by materials due to molecular vibrations • Vibration frequencies are influenced by • Atom Size • Environment • Bond Strength ….provides a vast amount of chemical information
Why Use Infrared Spectroscopy? Fourier Transform InfraRed (FT-IR) spectroscopy is an extremely powerful technique for identifying the molecular composition of many organic and inorganic materials. When analysed by infrared spectroscopy, materials produce a spectrum or fingerprint.