1 / 6

Recrystallization of para-dibromobenzene

Recrystallization of para-dibromobenzene. Recrystallization of para-dibromobenzene. Remove Insoluble Impurities Remove Soluble Impurities Isolate Solid by Removing Trace Amounts of Solvent. Solvent ; Dissolve solid when hot, but solid will recrystallize /solidify in cold solvent.

aquarius
Download Presentation

Recrystallization of para-dibromobenzene

An Image/Link below is provided (as is) to download presentation Download Policy: Content on the Website is provided to you AS IS for your information and personal use and may not be sold / licensed / shared on other websites without getting consent from its author. Content is provided to you AS IS for your information and personal use only. Download presentation by click this link. While downloading, if for some reason you are not able to download a presentation, the publisher may have deleted the file from their server. During download, if you can't get a presentation, the file might be deleted by the publisher.

E N D

Presentation Transcript

  1. Recrystallization of para-dibromobenzene

  2. Recrystallization of para-dibromobenzene • Remove Insoluble Impurities • Remove Soluble Impurities • Isolate Solid by Removing Trace Amounts of Solvent Solvent; Dissolve solid when hot, but solid will recrystallize/solidify in cold solvent.

  3. Remove Insoluble Impurities 1. Heat solid in minimum amount of warm solvent. Use a reflux condenser so solvent won’t evaporate. 2. Add activated charcoal to remove trace impurities. 3. Filter quicklywhile warm

  4. Remove Soluble Impurities • Slowly cool solution to room temperature to allow solid to recrystallize. • Put in refrigerator to make sure maximum amount of solid has recrystallized. • Filter to remove soluble impurities.

  5. Isolate Solid by Removing Trace Amounts of Solvent • Vacuum Filtration

More Related