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Overview of Vacuum Systems. Tejas Deshpande 24 July, 2014. Outline. Introduction Pumps Positive displacement pumps Momentum transfer pumps Entrapment pumps Pressure gauges Vacuum seals Manipulation and motion under vacuum. Introduction. Introduction: definitions.
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Overview of Vacuum Systems Tejas Deshpande 24 July, 2014
Outline • Introduction • Pumps • Positive displacement pumps • Momentum transfer pumps • Entrapment pumps • Pressure gauges • Vacuum seals • Manipulation and motion under vacuum
Introduction: definitions Kinetic Theory of Gases • Ideal gas equation • Velocity of molecules hitting chamber walls
Introduction: definitions Pumping • Rate of mass flow • Mass “conductance” http://fisica.ufpr.br/sharipov/tubefm.html
Introduction: definitions Pumping • Pump capacity & effective pumping speed • Rate of evacuation • Example: Pfeiffer Hena-25 pump + cylindrical chamber • Finite C with a hose
Introduction: definitions Pumping • Conductance of KF 40 hose (L = 10", D= 2.165") [1] [1]http://www.vacuumlab.com/Articles/Knowing%20Eff%20Pump%20Speed.pdf
Positive displacement pumps Rotary vane pumps • Principle of operation
Positive displacement pumps Scroll pumps • Principle of operation
Positive displacement pumps Diaphragm pumps • Principle of operation
Positive displacement pumps Roots “blower” • Principle of operation
Momentum transfer pumps Diffusion pumps • Air diffuses to vapor stream • Baffles condense vapor • Oil backstreaming problem
Momentum transfer pumps Turbomolecular pumps • Principle of a molecular “drag” pump • Mechanically similar to rotary pump • Good compression ratio • Poor pumping speed • Turbo pump
Momentum transfer pumps Turbomolecular pumps • Principle of operation
Entrapment pumps Ion pumps • Penning cell • Magnetic field acts as electron trap cyclotron orbits • Ions deposit on Cathode
Entrapment pumps Titanium sublimation pumps • Titanium as evaporatable “getter” material • Chemical sorption • 40-50 Ampere current evaporates Ti
Pressure gauges Liquid Manometers • Simplest U-tube manometer • Atmospheric pressure = 1 bar The Diaphragm Manometer • Capacitive sensor • AC vs. DC • DC capacitance bridge • AC resonant circuit tuned to diaphragm vibration
Pressure gauges Thermal Conductivity Gauges • Convection of heat through the gas • Other heat losses • Radiation ~ T4 • Solid conduction • Operating conditions • Free molecular flow • > 10-3torr
Pressure gauges Ion Gauge • Measurement of ion current • Gauge sensitivity • Bayard-Alpert gauge • Collector potential: -10 V • Grid potential: 180 V • Cathode filament: 30 V • Screen: 0 (ground)
Vacuum Seals O-ring seal • Elastomers, Viton-A, Polyimide • Quick and reusable • Limited baking range (< 250 °C) ConFlat flange seal • “Leak-tight” (< 10-12 Pa m3s-1) • Metal gaskets (typically copper) • Bakable to 450 °C • Not reusable
Manipulation and motion under vacuum Metal bellows • Mechanical feedthroughs • Bakable to 450 °C • Limited linear/angular stroke Continuous rotation • Speeds up to 2000 RPM • High torque bellows • Low torque magnets
Manipulation and motion under vacuum Gate Valve • Large bore • Sample transfer Right-angled valve • Small bore • Air evacuation
Manipulation and motion under vacuum Transfer arm • Significantly greater stroke than bellow-sealed manipulator • Magnetic power transmission
Summary • Introduction • Pumps • Positive displacement pumps • Momentum transfer pumps • Entrapment pumps • Pressure gauges • Vacuum seals • Manipulation and motion under vacuum