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One-Minute NMR: E-Seminar Protocols

One-Minute NMR: E-Seminar Protocols. As a courtesy to others, please mute your phone line while listening. Press *6 to mute (listen) Press #6 to un-mute (ask a question). One-Minute NMR 2007 Demo Tour. University of Buffalo: Buffalo, NY; January 8

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One-Minute NMR: E-Seminar Protocols

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  1. One-Minute NMR: E-Seminar Protocols As a courtesy to others, please mute your phone line while listening Press *6 to mute (listen) Press #6 to un-mute (ask a question)

  2. One-Minute NMR2007 Demo Tour • University of Buffalo: Buffalo, NY; January 8 • TriMR Regional Meeting: Research Triangle Park, NC; Feb 15-16 • Southwest Regional Demonstration, Kalypsys San Diego; March 27 • ENC: Daytona Beach, FL; April 22 – 26 • Schedule a live demo in your area! Call Protasis for details.

  3. One-Minute NMRWinter 2006-07

  4. 12th International Symposium on Marine Products Queenstown, New Zealand, February 2007 58 Speakers and Many Poster Presentations - Sponsors Included Protasis Corporation - • Sessions: • Discovery • Kirk Gustafson, National Cancer Institute, Frederick, MD • “Exploring the inherent chemical diversity of marine • invertebrates: New compounds from familiar sources” • Environment • Genome • Development • Barbara Potts, Neureus, San Diego, CA • “Marine microbe derived anti-cancer agents in Phase I clinical trials” • New Frontiers • William Fenical, Scripps Institute, San Diego, CA • “Marine natural products: Where we’ve been and where we’re going”

  5. Integrating NMR into Modern Laboratory Workflow The Wellplate and Microvial as Efficient Transport Media Among Automated Analytical Methods Data and Application Examples Courtesy of: • Professor John BluntUniversity of CanterburyChristchurch, New Zealand • Dr. David DetlefsenNovatia LLCMonmouth Station, NJ USA • Dr. Mike FreyJEOL, Peabody, MA USA • Mark O’Neil-Johnson Sequoia SciencesSt. Louis, MO USA

  6. Vacuum Centrifuge Mass Spec Wellplate-Centric WorkflowAn Example from the University of Canterbury HPLC Fract Collect Bioassay DAD ELSD NMR

  7. HPLC with ELSD detection of 600 mg extract of unidentified endophytic fungus E9,E10,E11 G4 250 mL/well

  8. 500 MHz 8 mg in 6 mL CD3OD PRESAT1.5 min Recognisable features: 5 CH3 groups, of which1 methoxyl, 3 singlet CH3-C,1 doublet CH3-C; 1 aldehyde

  9. only 1 hit 12

  10. MicroFlow NMR Literaturewww.microNMR.com

  11. Your MicroFlow NMR Product Sourcewww.protasis.com

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