LAB COURSE in GENERAL CHEMISTRY WS 2011

1. 8.11.2010 PRELIMINARY MEETING LAB COURSEinGENERAL CHEMISTRYWS 2011

2. Some organisational stuff Requirement: INTRODUCTION TO GENERAL CHEMISTRY 1 EINFÜHRUNG IN DIE ALLGEMEINE CHEMIE 1

3. Some organisational stuff CatchUp-Exam on Thursday

4. Some organisational stuff Is anyone here who actually doesn‘t want to attend the lab course?

5. Number of Workbenches • 64

6. Number of Workbenches How many students absolved the exam of „Introduction in General Chemistry 1“ in former years and want to attend this years lab course? • Lab? • Just Exam(s)?

7. Number of Workbenches HTL or similar practical education  You have to write the intermediate exams every Tuesday at 12.45 pm!  You don‘t have to do the practical work in the lab!  You have to write the final exam!

8. Number of Workbenches HTL or similar practical education? • Fill in on list • Copy of final certificate (until next week)

9. SUPERVISORS Dipl.Ing. Sebastian Leitner Dipl.Ing. Kerstin Oppelt Dipl.Ing. Lorenz Reith Dipl.Ing. Michael König Dipl.Ing. Eva Wöß Dipl.Ing. Christa Hirtenlehner

10. CONTACT DATA Office: TNF-Tower T533 Phone: +43 732 2468 9368 intern just 9368 Mail: eva.woess@jku.at Homepage: www.anorganik.jku.at

11. ATTENDANCE Our course is a so called PRACTICAL COURSE University law says: a practical course is a course with compulsory attendance and immanent exam situation

12. ATTENDANCE Physical presence is obligatory! • Noone who misses this lecture or the fire lecture can attend the lab course! • If you are ill, we need to see a doctors note! • Tell us BEFORE a lab day starts if you are ill -> CONTACT DATA!

13. SCHEDULE • Preliminary meeting today • Fire lecture and next week Place takeover • 5 weeks of lab work with intermediate exams • 1 week for work-up, cleaning and place returning • Final exam

14. SCHEDULE Exam in Introduction to General Chemistry 1 Preliminary Meeting Fire Lecture 1 Lab-week Tuesday-Thursday Place takeover 1st day Intermediate Exam 12.45 3 days of labwork Monday of the following Week until 12 am: PROTOCOLS T533 Lab-weeks Place cleaning and returning Final exam

15. SCHEDULE Labday 12.45-17:45 Uhr 12:45 – 13.00 Meeting with your supervisor in the Lab and discussion in groups of about 10 students + supervisor of todays labwork NO ONE STARTS ANY EXPERIMENTS BEFORE! TIME IS PRECIOUS – BE ON TIME 13:00 – 17:00 Uhr Labwork WE FEEL FREE TO CHECK YOUR KNOWLEDGE ABOUT CURRENT EXPERIMENTS! 17:00 – 17:45 Uhr Cleaning and Final check SIGN-OUT!

16. SCHEDULE

17. SCHEDULE

18. SCRIPTS & EXAMINATION MATTER www.anorganik.jku.at

19. SCRIPTS & EXAMINATION MATTER www.anorganik.jku.at

20. SCRIPTS & EXAMINATION MATTER • Guide for Laboratory in General Chemistry Praktikum aus Allgemeiner Chemie

21. SCRIPTS & EXAMINATION MATTER • Guide for Laboratory in General Chemistry Praktikum aus Allgemeiner Chemie

22. SCRIPTS & EXAMINATION MATTER • Guide for Laboratory in General Chemistry Praktikum aus Allgemeiner Chemie

23. SCRIPTS & EXAMINATION MATTER • Guide for Laboratory in General Chemistry Praktikum aus Allgemeiner Chemie • Primer (English) Primer (Deutsch)

24. SCRIPTS & EXAMINATION MATTER • Guide for Laboratory in General Chemistry Praktikum aus Allgemeiner Chemie • Primer (English) Primer (Deutsch) • Supporting Information: MSDS Laboratory Regulations Fire Issues PASSWORD

25. MARKING • Practical work • Protocols • Intermediate exams • Final exam

26. EXCLUSION CRITERIA • Experimental work: Insufficient practical work leads to exclusion from the laboratory course. Therefore a judging scheme exists: If you have to repeat a protocol you get one negative entry, if you have to repeat an experiment you get two negative entries. If the number of negative entries exceeds eight, you are excluded from the laboratory course. • Behaviour: A major offense against the laboratory regulations leads to exclusion from the laboratory course. A minor offense against the regulations leads to a negative entry in the “don’t exceed the eight entries”-scheme mentioned above! • Weekly exams: If you fail twice in the weekly exams you are excluded from the laboratory course.

27. Download: On our HP in English and German! Read it, obey it! Next week you have to sign a list: “With your signature you confirm your participation at the lab course “Laboratory in General Chemistry” and you accept the laboratory rules!” LABORATORY REGULATIONS

28. You need a (big) book for laboratory protocols which you have to write by hand, and a laboratory journal (small book) for notes in the lab. No practical guide is allowed in the lab! How to write a protocol will be discussed during labcourse! LABORATORY PROTOCOLS

29. LaborORDNUNG / TIDYNESS WRONG! CORRECT! Bottles and flasks marked with content name and place number (permanent marker) Removed dirty glassware that is not longer use Closed chemical containers

30. Lab coat Lab goggles Suitable gloves Long hair tied together SAFETY CLOTHING

31. Cleaning equipment (sponge, cleaning agent, kitchen paper) Permanent marker Calculator Lab journal Protocol book LAB EQUIPMENT Lab coat Safety goggles Spatulas (big and small) Peleus ball Gloves (butyl nitrile, neoprene)

32. Cleaning equipment (sponge, cleaning agent, kitchen paper) Permanent marker Calculator Lab journal Protocol book LAB EQUIPMENT Lab coat Safety goggles Spatulas (big and small) Peleus ball Gloves (butyl nitrile, neoprene) Sold at Laboratory Place Takeover!

33. Cleaning equipment (sponge, cleaning agent, kitchen paper) Permanent marker Calculator Lab journal Protocol book LAB EQUIPMENT Lab coat Safety goggles Spatulas (big and small) Peleus ball Gloves (butyl nitrile, neoprene) You need your full equipment each Lab-work-Day starting with 22.11.2011!

34. EMERGENCY NUMBERS ● Portier (internal phone call) 9100 ● fire brigade: 8122 (internal phone) ● police: 8133 (internal phone) ● ambulance: 8144 (internal phone) ● 112 (EU emergency call) ● cell phone: 0732/2468 8122 (e.g.)