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Wed. evening (Mar. 28) Expt.21; finish 16 Thurs. afternoon (Mar. 29) Expt. 21; finish 16

Wed. evening (Mar. 28) Expt.21; finish 16 Thurs. afternoon (Mar. 29) Expt. 21; finish 16 Fri. afternoon (Mar. 30) Expt. 21; finish 16 Mon. afternoon (Apr. 2) Expt. 21; finish 16 Mon. evening (Apr. 2) Expt. 21; finish 16. Menthyl chloride. + H2O.

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Wed. evening (Mar. 28) Expt.21; finish 16 Thurs. afternoon (Mar. 29) Expt. 21; finish 16

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  1. Wed. evening (Mar. 28) Expt.21; finish 16 Thurs. afternoon (Mar. 29) Expt. 21; finish 16 Fri. afternoon (Mar. 30) Expt. 21; finish 16 Mon. afternoon (Apr. 2) Expt. 21; finish 16 Mon. evening (Apr. 2) Expt. 21; finish 16

  2. Menthyl chloride

  3. + H2O

  4. The lower boiling points of the alkene products relative to the alcohols, makes it possible to distill over an alkene/water mixture as they form.

  5. How would you use NMR integration to calculate relative percentages of components in a mixture?

  6. How do you choose which hydrogens to integrate?

  7. The integration areas of isolated hydrogens can be used to calculate relative percentages of components in a mixture.

  8. Calculating Percentages using Integration areas

  9. Simulated 1H NMR spectrum of 1-methylcyclohexene

  10. Simulated 1H NMR spectrum of 3-methylcyclohexene

  11. Simulated 1H NMR spectrum of 4-methylcyclohexene

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