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PIPOC 2007, Malaysia

PIPOC 2007, Malaysia. Detergent Complex Based on Palm Stearin. August 29, 2007. Agenda. About Trivedi Group Basic Requirements and Process Chemistry Products and Formulations Cost Structure Summary. Global Changes call for Action Now!. Hurricanes and natural disasters

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PIPOC 2007, Malaysia

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  1. PIPOC 2007, Malaysia Detergent Complex Based on Palm Stearin August 29, 2007

  2. Agenda • About Trivedi Group • Basic Requirements and Process Chemistry • Products and Formulations • Cost Structure • Summary

  3. Global Changes call for Action Now! Hurricanes and natural disasters Global warming Fossil vs. Renewable Food vs. Fuel

  4. Organization Chart

  5. Chemithon Engineers Pvt Ltd • Sulfonation of alkylates • Environmental Systems TECHNOLOGY & ENGINEERING • Trivedi Industrial Research & Associates • Oil Seeds Plantation • Edible Oil/ Solvent Extraction • Esterification & Fractionation Processes • Detergent and HPC production • Ethoxylation & Hydrogenation • Glycerin Purification • Pilot Plant Studies

  6. Anionics Amphoterics Cationics SURFACTANT MANUFACTURING Custom Blends Nonionics Specialities

  7. Palm Derivatives Alcohols Surfactants Soap Noodles Specialities Detergent Alkylates Zeolites Ethoxylates CHEMICAL TRADING

  8. Business Promotion (NRDC) • Market Studies PROJECT SERVICES • Project Appraisal (IFC) • Feasibility Studies • Project Co-ordination • Energy Audit

  9. CPO with 5% FFA (1000 MT) Extraction Vitamin E (1.5 – 2.0 MT) Refining PFAD (65 MT) Fractionation RBD Palm Stearin (185 MT) RBD Palmolein (745 MT) Requirements for Palm Plantation Based on Bio-Refinery • Minimum Area: 60.000 Hectares • FFB • CPO: 1000 TPD • PKO: 100 TPD Mass Balance

  10. A detergent based complex of Palm Stearin creates tangible advantages • Sustainable value creation from Palm Stearin • Independent revenue platforms • Pharmaceuticals (Glycerine) • Fuel (Biodiesel – C18 rich) • Alkylates (C12-14, C16) • Detergents and Home & Personal care products • Based on renewal resource • Environmentally friendly project

  11. RBD PS (185 MT) Transesterification Glycerine (18 MT) C1214 Ester (2.5 MT) C16 Ester (110 MT) C18 Ester (71 MT) Distillation Hydrogenation Amidation / Amides Ethoxylation / ME Ethoxylates Sulfonation MES (145 MT) Blending / Drying HPC Products Detergents (725 MT) Typical mass balance highlighting various steps in the process

  12. CH2-OOC-R1 CH2-OH R1-COO-R’ Catalyst CH-OOC-R2 + 3R’OH R2-COO- R’ + CH2-OH @ 60 - 70˚C CH2-OOC-R3 R3-COO- R’ CH2-OH Step 1: Transesterification step converts a triglyceride to esters and glycerol Triglyceride + Alcohol Esters + Glycerol

  13. Step 2: Distillation of fractions is done via a three stage conversion column C1214 C16 C18

  14. Step 3: A continuous fixed bed column is used for hydrogenation step

  15. METHYL ESTER 1V0.1 SULFONATION DIGESTION BLEACHING MeOH RECOVERY NEUTRALIZATION DRYING METHYL ESTER SULFONATES (MES) (>85% ACTIVE AND <5% DISALT) Step 4: Sulfonation of esters yields methyl ester sulfonates (MES)

  16. Sulfur (95) SO3 gas generation C16 methyl ester (662) Sulfonation Methanol Recovery MESA digestion Methanol Makeup (40) 50% H2O2(35.6) MESA bleaching Distillation (226) 50% Caustic (242) Neutralization Drying MES kg MES 843 Di-salt 49 Sodium methyl sulfate 50 Unsulfonated 20 Na2SO4 10 Moisture 26 Hydrogen Peroxide 1 Methanol 1 Total 1,000 C16 MES(MW 372) has the typical mass balance as shown in the flowsheet

  17. STILL AWAKE???

  18. Palm Kernel C8-c18 Coconut C12-C14 Palm Stearin C16-C18 Soya C18 Tallow C16-C18 Different forms of MES dried and stripped can be obtained as final product

  19. Some pictures of the Huish Plant

  20. Flowsheet for Detergent Powder Plant

  21. Typical Components in a Detergent Formulation

  22. Huish products are used in a variety of products both powder and liquid

  23. Typical Components in a Soft Soap Formulation

  24. Different Products containing MES in their formulation

  25. Typical capital expenditure for a palm based detergent complex is about $ 50 million

  26. Estimated costs for esterification, distillation and MES production

  27. Estimated production costs for soft soap and detergents

  28. Project provides multiple advantages across different platforms • Integrated complex with optimum value addition • Sustainability using renewable raw materials • MES in dry flakes form - convenience of use • Biodiesel EN 14214 compliant (summer grade) • Independent revenue platforms

  29. Thank You! “ The best way to predict the future is to create it” Address: SHIV ANAND-A 1ST FLOOR, 372/374 S. V. ROAD, GOREAGAON (W) MUMBAI - 400 104 INDIA Website: www.trivedigroup.com Email: strivedi@trivedigroup.com

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