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Produce Water Analytical Field Trials and Methodology Development

Produce Water Analytical Field Trials and Methodology Development. SPE: Reducing Environmental Impact of Unconventional Resource Development 23 – 25 April 2012 San Antonio, Texas | Omni La Mansión del Rio. A Joint Effort. Texas Engineering Extension Service GPRI /TEES/TCAT/TAMU-PE

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Produce Water Analytical Field Trials and Methodology Development

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  1. Produce Water Analytical Field Trials and Methodology Development SPE: Reducing Environmental Impact of Unconventional Resource Development 23 – 25 April 2012 San Antonio, Texas | Omni La Mansión del Rio

  2. A Joint Effort Texas Engineering Extension Service GPRI/TEES/TCAT/TAMU-PE University Alliance TAMU-SRPH GSI Environmental MI-SWACO Oil & Gas Industry Partners

  3. Goals Establish Analytical Background Data Focus on New Protocols and Instruments Method Modifications Enhanced Sampling Techniques Treatment Monitoring Collect Scientific Data of Produced Waters

  4. Treatment and R&D On-Site Membrane Desal-Laboratory

  5. Sampling the Various Treatment Streams

  6. Interior Space

  7. Analyses pH, Turb. Cond., TS, BTEX, Hard, Ions (Cat. & An.), O&G, TOC, Alk., Chlorides Bacteria Scan Isotopes Metals Others (i.e. Methane)

  8. Notable Background Results

  9. New Protocols & Techniques HACH Frac-Water Kit

  10. HACH Kit Wet-Chemistry Methods Chloride ISE & HQ40D Meter Pilot Tested Protocols Sample Prep Adjustments Noted Matrix Interferences

  11. Since Then HACH Has the New Kit On The Market Issues Noted in Trials Were Corrected Adjustments to Chemistries Documented Methods Redesigned and Written

  12. InnovOx

  13. GE Analytical InnovOx SCWO TOC/NPOC Originally Designed for Industrial Waste Monitoring & Sewage Analyses Brought It To The “Next-Level” First Major Field Trial Researched the Overall Method and Performance of SCWO on Produced Waters

  14. Since Then Modified Sparge Chamber 30 New Chemistry Protocols for Produced Waters Redesigned Software Newly Designed Acid Flow Ratio Valve TEEX: “Go-To” People for TOC/NPOC Analyses of Produced Waters

  15. Hapsite GC/MS for BTEX/VOC

  16. Inficon-HAPSITE GC/MS First Time in Field Analyzing Produced Waters Primarily Used in Air Quality Monitoring and Military Monitoring Preliminary Modifications Planned for Before Deployment What Issues Could Arise?

  17. Hapsite Great First Trial Accuracy & Precision Were On-Target No Issues With Sample Matrix Noted Since: Working on Research and Usage Concepts

  18. Additional Evaluation Studies Modified Oil & Grease Methods TPH Scan Future Concepts of On-line analysis Instruments Improving Upon Existing Methods Developing Specifics for Industry Clients

  19. Isotopic Sample Kits

  20. Radioisotope Success! Results Very Important to Treatment Process & Monitoring Builds Strong Database of Water Quality Not Existing Provides Additional Understanding to Important Research and Treatment Steps

  21. Future of Analytical Monitoring of PW Additional R&D Needed Research Prospects for Analytical Roundtable Group Enhanced Scientific Collaborations Developing Extensive Background Data of Waters Sharing of Scientific Results

  22. Thank You! Keith McLeroy Associate Training Specialist W/WW TEEX and Analytical Advisor, to GPRI TEEX-Water & Environmental Program Keith.mcleroy@teexmail.tamu.edu 979-458-0912

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