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A new System for Single Particle Strength Testing of Grinding Powders. Einar List Joerg Frenzel Heiner Vollstaedt. AfraTest – not only for diamond. A brasive Powders Fra cture Strength Test er. Content. The specimen General machine layout Find, measure and pick the particle
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A new System for Single Particle Strength Testing of Grinding Powders Einar List Joerg Frenzel Heiner Vollstaedt
AfraTest – not only for diamond • Abrasive • Powders • Fracture • Strength • Tester
Content • The specimen • General machine layout • Find, measure and pick the particle • Place and crush the particle • Interpretation of the force / time plot • Results • Outlook
Small and tough – a challenge • Sizes from 1000 µm down to 46 µm • Extremely wide fracture strength range • Automatic handling, new anvil for every particle
Digital image processing • Particle size (whatever this means) • Particle Shape • Position • Proximity to neighbours?
Particle size • Minimum feret diameter
Particle size • Minimum feret diameter • Maximum feret diameter
Particle size • Minimum feret diameter • Maximum feret diameter • Area
Particle size • Minimum feret diameter • Maximum feret diameter • Area • Area equivalent circle diameter
Shape • Compactness calculated from Perimeter and Area
Shape • Roughness • Convex Outline
Position • Centre of gravity • Surrounding box • Surrounding box + safety distance must be empty
Shape • Moments of inertia • Minimum and maximum moment of inertia • Ellipticity
Images ready for processing 1.2 µm per pixel 4.5 µm per pixel
Find and pick the particle • Particles on a glass plate • Monochromatic lighting • Autofocus optics • Sample holder mounted on a planar drive
Place and crush the particle • 300 mm moveable anvil bars • 2000 N and 200 N range • 16 bit force resolution • 10,000 samples/s • Offset and excitation compensation
Which fracture force? For now we take the first fracture.
Influence of the anvils • Indentation of the anvil • Lower anvil hardness causes higher fracture forces of the particles • Usage of different anvils for the same powder? Footprints of 55µm diamonds on WC anvils (z~10 µm)
Do we know the fracture stress? The true Area A under stress is unknown! We don´t know the true stress! As imperfect as it is:we calculate CFS using the particle cross section area or the area of the inscribed circle
Conclusions and outlook • AfraTest can handle the size range from fine powder to coarse grit • The measuring range allows for testing superabrasives as well as conventional abrasives • The first fracture is suitable for comparing materials. • A compressive fracture strength can be derived, making different assumptions for the loaded area. • AfraTest produces results on a common scale for abrasives and superabrasives.