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Plasma Cleaner. Instructions for Use. Fischione 1020 Plasma Cleaner. General. Most of the cleaning process with the 1020 are automatic. The process is started by entering a cleaning time.
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Plasma Cleaner Instructions for Use
General • Most of the cleaning process with the 1020 are automatic. • The process is started by entering a cleaning time. • Once the process starts the specimen chamber will automatically pump and initiate plasma cleaning. The chamber will remain under vacuum until vented by the user. • VENTING TAKES 3 – 4 MINUTES. TURBO PUMP MUST SPIN DOWN.
Gas Supply • Make sure the gas supply is on and there is gas. • Gas is an Argon – Oxygen mixture. • NOTE, just check the gauge. Do NOT adjust ANY valves.
Check Control Panel • Normally the specimen holder will be under vacuum. • First check the control panel. • If the “HIGH VACUUM” light is illuminated, you must vent the specimen chamber.
Venting the Specimen Chamber • Press VENT on the control panel. • The VENTING LED will illuminate. • It takes 3 – 4 minutes to vent the chamber.
Chamber at Atmosphere • Wait until the ATMOSPHERE LED is illuminated before opening chamber.
Remove the plug • After the chamber is vented, remove the plug from the TEM specimen port. • Place the plug in the plastic bag on top of the plasma cleaner. • The chamber is now ready for insertion of the TEM specimen holder.
Insert TEM Specimen Holder • Insert the TEM specimen holder into the chamber. • The specimen holder may come to a stop but may not be fully inserted (see image). Do not push on the specimen holder at this time. WAIT.
Set Cleaning Time • Using the number pad on the control panel input the cleaning time. Cleaning time for most TEM specimens is 30 sec to 5 minutes. • Press SET to start the pump down and cleaning cycle.
Check Holder and Clean Cycle • When the pumping cycle starts the holder should then move into the specimen chamber. CHECK THIS. • When cleaning is underway, the gas mixture will luminesce. This can be observed through the window.
Clean cycle end and vent • The timer will count down as the cleaning cycle continues. At zero cleaning will end but the chamber remains under vacuum. • To Vent, press VENT. • REMEMBER: 3 to 4 minutes to vent chamber.
Shut Down # 1 • Remove the holder from the specimen chamber. • Replace the Plug
Shut Down # 2 • Press PUMP to pump down the chamber. • Chamber is left under vacuum • Wait and make sure the chamber returns to HIGH VACUUM
APPENDIX • An accessory is available for inserting SEM stubs (FEI type). • A vacuum pumping station for TEM holders is also avaible.
Remove the TEM Port • The TEM port must be removed before the SEM specimen holder can be placed in the cleaning chamber. • Unscrew the black retaining ring and remove. • Take out the TEM port and place on a clean surface. Be careful of, and check the large O-ring
Insert the SEM specimen holder • Insert the SEM specimen holder. Be careful of the large O-ring. • The holder sits flushin the opening when fully inserted.
High Vacuum Docking Stations • TEM holders can be kept under vacuum in the TEM Docking station. • To use: • Contact CAF personnel.