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. Instrumental Analysis of Volatile Compounds. Static headspace analysis Dynamic headspace analysis Solid phase microextraction. . Detection Limits and Reproducibility of Organic Volatile Compounds in Water. . Definition of Solid Phase Microextraction. Equilibrium partitioning of the compounds between the coating fiber and sample or headspace..
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1. Solid Phase Microextraction Analyses of Flavor Compounds in Foods David B. Min
Department of Food Science and Technology
The Ohio State University
Columbus Ohio
3. Detection Limits and Reproducibility of Organic Volatile Compounds in Water
4. Definition of Solid Phase Microextraction
5. Diagram of SPME Extraction
6. Principles of Headspace SPME
7. SPME Analysis of Volatile Compounds
8. Types of Solid Phases
9. Effects of Different Solid Phases on the Hexanal Analysis in Soybean Oil
10. SPME Reproducibility of Major Flavor Compounds in Orange Juice
11. Effect of Injection Temperature on Chromatograms of Soybean Oil Volatile Compounds
12. Effect of Coating Thickness on the Absorption for the Extraction of 0.1 ppm Benzene
13. Effect of Distribution Constant on the Absorption Profile of 0.1 ppm Analyte
15. Effect of Water and Microwave Heating on the chromatograms of Headspace Polyaromatic Compounds
16. Effect of Stirring Rate on the Extraction of 1 ppm Benzene in Water
17. Effect of Agitation Method on the Extraction of 1 ppm Benzene in Water
18. Effect of Benzene Concentration on Extraction by SPME
19. Effect of Salts on the Extraction of Volatile Compounds by SPME
20. Matrix Effect on the Extraction of Alcohols by SPME
22. Regression Equations between Flavor Compounds (ppm) and GC Peak Areas
23. Effects of Temperature and Time on the Equilibrium of Flavor Compounds Between the SPME Coating and the Headspace of Orange Juice
24. Isolation Time Effect on Soybean Oil Volatile Compounds by SPME
25. Isolation Temperature Effect on Soybean Oil Volatile Compounds by SPME
27. Volatile Compounds in the Headspace of Soybean Oil by SPME-GC-MS
28. Effect of Isolation Temperature on Corn Oil Volatile Compounds by SPME
29. Volatile Compounds in the Headspace of Corn Oil by SPME-GC-MS
30. Chromatograms of Soybean Oil and Corn Oil
31. Factors for the Sensitivity of Solid Phase Microextraction
32. Conclusion