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CHEMICAL LABORATORY. Jan Michalíček Jitka Herzogová Faculty of Chemistry Brno University of Technology 2005. What‘s a chemical laboratory?. a place for special researches different kinds of laboratories (analytical, physicochemical, organic, inorganic, etc.) necessary equipment
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CHEMICAL LABORATORY Jan Michalíček Jitka Herzogová Faculty of Chemistry Brno University of Technology 2005
What‘s a chemical laboratory? • a place for special researches • different kinds of laboratories (analytical, physicochemical, organic, inorganic, etc.) • necessary equipment • safety instructions must be kept there
Alchemist laboratory - basic equipment - metal shears - filtering vessel - casting mould - vessel for separating oils lighter than water - crystallising dish - vessel for separating oils heavier than water - glass funnel vessel [vesәl] nádoba shears [šiәz] velké nůžky, kleště casting mould [ka:stiŋ mәuld] licí forma funnel [fanl] nálevka
Alchemist laboratory - basic equipment - iron pots for strong acids - casting ladles - crucibles - troughs for gold-washing casting ladle [ka:stiŋ leidl] slévačská pánevcrucible [kru:sibl] kelímek trough [trof] žlábek, korýtka
Alchemist laboratory Elements: I. Oxygen 2. Hydrogen 3. Nitrogen 4. Carbon 5. Sulphur 6. Phosphorus 7. Gold 8. Platinum 9. Silver 10. Mercury11. Copper12. Iron13. Nickel14. Tin15. Lead16. Zinc17. Bismuth18. Antimony19. Arsenic Compounds:37. Water43. Nitric acid44. Nitrogen peroxide 45. Nitrous acid47. Carbon dioxide50. Sulphuric acid53. Ammonia54. Ethylene55. Methane57. Compounds of sulphur and hydrogen Edward Kelly (1555–1597) Dr. Dee
Alchemist laboratory Images of alchemical apparatus of distillation
Modern laboratory - equipment • from porcelain, plastic and metal material:mortar and pestle, Buchner funnel, crucible, tong, spoon • glassware: pipette,beakers,flasks,burets, funnels, watch glass, test tube… • chemicals buret [bjuə’ret ] byreta flask [fla:sk] baňka funnel [fanl] nálevka pipette [pi’pet] pipeta
Modern laboratory - equipment • Sophisticated laboratory devices: NMR and massspectrometers UV-VIS spectrophotometers chromatographs Analytical balance
What we have to do... • to prepare for every laboratory session • to work quickly but correctly • to calculate and work up results of measurements • our results write down a report …to get credits
Do you conform to the safety rules? • Wear safety clothes (shroud) and gloves if it’s necesary! • Use glasses or a security shield! • Respect all instructions! or…
Useful web pages http://www.alchemy.cz/museum.htm http://www.levity.com/alchemy/songverd.htmll http://cs.wikipedia.org/wiki/Alchymie