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Status Report: Experimental investigation of beryllium. October 2014

This report details the experimental investigation of beryllium conducted in October 2014 at the University of Oxford, UK. The research includes examinations of the as-received beryllium, proton irradiation, ion irradiation experiments, microstructural investigations, and micromechanical tests. Characterization methods such as SEM, EDX, EBSD, TEM, and APT were utilized to study grain size, texture, precipitates, and dislocation structure. Plans for future tests, such as nanoindentation and ion irradiation, were outlined. Various steps in sample preparation and data quantification were discussed, along with the progress and upcoming tasks related to the research project.

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Status Report: Experimental investigation of beryllium. October 2014

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  1. Status Report: Experimental investigation of beryllium. October 2014 Viacheslav Kuksenko, Steve Roberts University of Oxford, UK

  2. Experiments: Investigation of the as-received Be Investigation of the existing proton Be windows - “real” GeV proton irradiation; • irradiated volume is big enough for microstructural investigations and micromechanical tests Simulation with ion irradiation experiments - flexibility of irradiation conditions - observations of the evolution of the microstructure; - reasonable correspondence of He/dpa ratio. Low energy in-situ irradiation: • easy variation of irradiation parameters; High-energy irradiation + PIE • microstructural and micromechanical tests data will be available

  3. Characterisation of as-received Be PF-60/VHP SEM 20 µm Oxygen Aluminium Grain size Texture Precipitates Dislocation structure SEM + EDX + EBSD 0.15 TEM ( + APT) 0.10 Fraction 0.05 30 20 0 10 Grain size (diameter), µm

  4. Characterisation of as-received Be • Samples preparation • Mechanical polishing lab is organised. • Polishing procedure up to “EBSD quality” is developed. • PF60 – 4 samples are polished. • S200F – 4 samples are polished. • EDX and EBSD • PF60 – experiment are made. Quantification of the obtained results should be finished. • S200F – will be characterised after the surface contamination test result. • TEM and APT – FIB at CCFE should be used. • FIB trainings are finished. “Driving test” is next week. • Be sample will be transferred to CCFE next week for the contamination test. • Plan to start FIB of Be in late October – beginning of November • Nanoindentation • will be made after the nano-indenter repairing EBSD 35 µm

  5. 300 kW NuMI beam window (MARS calculations of Brian Hartsell, Fermilab) • 120GeV proton beam • about 3×1013 protons per pulse, 0.5 Hz • 1.57×1021 protons during its lifetime • 1.1mm beam sigmas, X and Y • T ≈ 70ºC 300 kW NuMI beam window The window can be accepted by the University. Will be shipped from Fermilab soon 1) to determine the exposed area by the dosimetry film. 2) SEM + EDX characterisation. 3) nano-indentation (nano-indenter doesn’t work now). Then – transfer to CCFE for FIB samples preparation. This year December-January?

  6. Low energy ion irradiation: • FIB samples preparation at CCFE should be started. • Be sample will be transferred to CCFE next week for the contamination test. • Next step: preparation of samples. This year. • High energy ion irradiation: • mechanical polishing procedure is developed; • irradiation conditions are determined (multi-energy implantation). • aluminium coating of the test sample (non-toxic) is delayed due to the technique failure. No updates since mid of September.

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