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NHMFL High B/T Facility - Gainesville. ENHANCEMENTS 2008-2009 I. Completed addition of 10T-10 mK facility --- annex to Microkelvin Laboratory fast turn-around, test samples, cells prior to use in ultra-low temperature
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NHMFL High B/T Facility - Gainesville ENHANCEMENTS 2008-2009 I. Completed addition of 10T-10 mK facility --- annex to Microkelvin Laboratory fast turn-around, test samples, cells prior to use in ultra-low temperature High B/T Facility (0.25mk, 16 T) II. Extended NHML user to Bay 2 of Microkelvin Laboratory (0.05mk, 8T). Seeking research scientist to provide needed staff III.In Progress: New 20T magnet (Cryomagnetics Inc.) Aug. completion of inner-most Nb3Sn insert coil Sep. completion of all Nb3Sn coils Oct. Completion of 20 T and demag coil set Nov.-Dec. Final assembly and testing Delivery ---- end of Dec. 2009
Scientific Mission of the Facility Dedicated to high-B experiments requiring T< 20 mK Experiments generally require a quiet environment and/or a long coolingtime. High Magnetic Field B = 15.3/16.5 T ( upgrade to 20 T, 2009 Homogeneity 1.6x10-5 10 mm DSV < 3x10-3 over 100 mm axial length 30 mm-dia bore, 25 mm-dia experimental space Ultra-Low Temperature 5 mole PrNi5 (nuclear refrigerant), Tmin < 0.4 mK 8 nW cooling power, t > 6 weeks @ 1 mK (world’s largest) CAPABILITIES:Method for Highest B/T
Capabilities and Specialized Instruments Electrical Transport Measurements High frequency Pulsed NMR (300 MHz – 1.6 GHz) Ultrasound High sensitivity bridges Vibrating-wire viscometers Sample rotator (–10 to +90, with a liq-3He actuator) Low temperature RF pre-amplifier -- NMR applications Thermometry Pt NMR T < 20 mK, in low B space 3He melting curve thermometer 0.4 mK < T Vibrating-wire thermometer 1.7 mK < T Kapton capacitance thermometer 4 mK < T CMN susceptibility thermometer 15 mK < T, in low B space RuO2 resistor (all commercial) 20 mK < T, in low B space Instrumentation
Rotator sample rotator heat exchanger HIGH B/T CAPABILITIES: Ultra-Low T ROTATOR
HIGHB/T CAPABILITIES: NMR Cell HIGH B/T Instruments: NMR Cell NMR up to 16 T : Studies of quantum diffusion of 3He in superfluid 4He for high nuclear spin polarization. Re-entrant cavity with walls at relatively high temperature and sample in cold finger inside cavity
NEW CAPABILITIY: LOW TEMPERATURE AMPLIFIER HIGH B/T Instruments: NMR Cell Uses HEMT transistor (simple source follower) can operate to ~ 0.3 K T Noise ≤ 1 K C. Huan, et al. J. Low Temp Phys. (in press) First application: low frequency NMR at ultra-low T
Crossed-Coil NMR Probe: low frequency, low gamma S. S. Kim, C. Huan et al. J. Low Temp. Phys. (in press) amplifier standoffs NMR cell Pulse B1, create transverse Magnetization in receiving coil
2008-2009 Users and Experiments • 1. FQHE of n=5/2 and 7/2 States in High Density Sample. • W. Pan (Sandia Nat. Lab.), D.C. Tsui (Princeton) • 2. Supersolid4He and NMR of 3He Impurities • D. Candela et al. (U. Mass.). • 3 & 4. BEC and Quantum Phase Transitions in S=1 Antiferromagnet. • V. Zapf et al. (LANL) • 5. Charge Carrier Density Variation 5/2 Fractional Quantum Hall Effect • W. Pan (Sandia )D. Tsui (Princeton University) • Systematic investigation of the metal-insulator transition at • ultra low temperatures in p-type GaAs FET structures. • D. Luhman, D.C. Tsui (Princeton Univ.) • 7. Magnetic Interactions of Novel Materials at Low T/High B. • M.W. Meisel (UF), A. Feher et al. (Šafárik Univ., Košice, Slovakia). • 8. Search for long-range magnetic order in weakly coupled quantum S=1/2 chain system • T. Hong and A. Zheludev, NSSD, ORNL • High sensitivity dielectric measurements supersolid 4He • M. Chan et al. Penn State U. Bay 3 Bay 3 Bay 3 & Wm Annex Bay2 Wm Annex Wm Annex Wm Annex
2009 Future Users and Experiments • 1. Magnetization Studies of NFL Ground State of CeCoIn5 • A. McCollam & S.R. Julian (U. Toronto) • Dielectric susceptibility studies of supersolid 4He • M. Chan, (PSU), L. Yin et al. (UF) • 3. Search for Half-Metallic Ground State in Quasi-One Dimensional Magnet • Xiao-Dong Wen, Thomas J. Cahill, Roald Hoffmann (Cornell) Bin Zhang (Chinese Academy of Sciences) • 4. Studies of Magnetic PN Junctions . • N. Rangaraju, B. Wesson (NthWestern Univ.) • 5. Quantum Tunneling in Molecular Magnets • N. Dalal (FSU) • 6. Two-dimensional metallic states –GaAs Quantum Wells) • S. Tozer et al. (FSU, NHMFL) • 7. High B Studies of Paramagnetically Doped materials • M.H. Levitt, Univ. of Southampton) Bay 2, Oct. 09 Wm Hall Annex, Sep. 09 Bay 3, Jan.? 09 Interest/Proposal Pending Request/Proposal in Prep. Interest/Proposal Pending Interest/Proposal Pending
Science Highlights 1 NMR Studies of Dilute 3He in Solid 4He and Test of proposed Supersolid state. D. Candela (Univ. of Massachusetts),Sung Su Kim, Chao Huan, Liang Yin, Jian-sheng Xia et al. University of Florida and NHMFL. NMR measures quantum tunneling of 3He impurities in solid 4He: Low T values of T2 give 3-4 quantum exchange rates: Strongly dependent on impurity concentration interaction V=Vo/Rn short range -- best fit long range Support: NHMFL Collab. Grants Res. Program S. S. Kim, C. Huan et al., J. Low Temp. Phys. (in press)
Science Highlights 2 Interplay of Frustration and Magnetic Field in 2D Quantum Antiferromagnet A. Orendáčová et al., University, Košice, Slovakia; M. W. Meisel et al., NHMFL. Cu(tn)Cl2 (tn = C2H10N2): S = ½ anisotropic 2D highly frustrated magnet: square lattice with nn J (= 3 K), frustrating nnn J′ (< 0.6 J), weak interlayer J′′ (~ 10−3 J) Max. peak Heat capacities structure idealized Test BKT model for ideal square lattice: vortex-antivortex (V-AV) binding at low T,B with transition to spin gap at Bsat A. Orendáčová et al., PRB (submitted), arXiv:0906.3181 BKT calculation (Cuccoli et al. PRB 68 (2003)). χac at NHMFL-UF Wm 123 Facility. All other symbols from Cv analysis. Acknowledgements: VEGA (1/0078/09, APVV-0006-07), ESF RNP , NSF DMR-0701400, DMR-0654118, State of Florida, Deutsche Physikalische Gesellschaft (DPG), EuroMagNET II, US Steel Košice s.r.o. High B/Low T susceptibility measurements
Bose-Einstein Condensation Universality Class NiCl2- 4SCs(NH2)2 at Ultra-Low T V.S. Zapf L. Yin et al. , A. Padhuan-Filho Ni S=1 spins: 3D XY anti-ferromagnet --- critical fields: Hc1 ~ 2 T, Hc2 ~12 T. Expectpower-law T dependence: Hc1(T) -- Hc1(0) = aT with = 1.5 Confirmed at mK temperatures with a=1.470.01 Unit cell of tetragonal NiCl2–4SCs(NH2)2 Science Highlights 3 AC susceptibilty measurements, NHMFL High B/T facility L. Yin et al., Phys. Rev. Lett. 101,187205 (2008)
Disorder driven gapless superfluid in high porosity aerogel : Ultrasound measurements Y. Lee et al., Phys. Rev. Lett. 98, 225301 (2007). Science Highlights 4 Tunneling exp. cannot be done for superfluid. BUT w-dependence of ultrasound attenuation can provide similar info. ? Sharma and Sauls, Physica B (03)
Growth of Users and CostsHigh B/T Facility (2005-2009 Liquid helium costs (k$) No. Users/Yr added part Bay 2 Support (10 k$)
Personnel High-B/T Personnel • Program Manager: Jian-Sheng Xia ………….U.F. Res. Scientist • Postdoctoral Assoc: Liang Yin………………...NHMFL supported • Bay 2 Manager: Naoto Masuhara…............U.F. Engineer • Program assistant: Darlene Latimer…………U.F. Staff • Microkelvin Lab Director : Neil Sullivan ……….U.F. Faculty • Affiliated faculty (Physics): • Gary Ihas • Yoonseok Lee • Mark Meisel • Neil Sullivan • Yasu Takano • Jian-sheng Xia