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LABORATORY NOTEBOOK (Pre-lab)

LABORATORY NOTEBOOK (Pre-lab). TITLE AND DATE OBJECTIVES TABLE OF PHYSICAL DATA Include the MW, bp, density, and hazard information for 2-bromoheptane, cis-2-heptene, trans-2-heptene, 1-heptene, methanol, and t-butanol.

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LABORATORY NOTEBOOK (Pre-lab)

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  1. LABORATORY NOTEBOOK(Pre-lab) • TITLE AND DATE • OBJECTIVES • TABLE OF PHYSICAL DATA • Include the MW, bp, density, and hazard information for 2-bromoheptane, cis-2-heptene, trans-2-heptene, 1-heptene, methanol, and t-butanol. • Include the MW, mp, and hazard information for sodium methoxide and potassium t-butoxide. • CHEMICAL EQUATION • Include the general chemical equation from page 99. • PROCEDURE • Include a brief outline of the procedure for the experiment. Do NOT copy directly from the lab manual. • Include a reference to the lab manual including page numbers where the actual procedure can be found.

  2. LABORATORY NOTEBOOK(In-lab) OBSERVATIONS/CALCULATIONS • Identity of base and solvent pair • Initial weight of 2-bromoheptane • Initial weight of base used • Initial volume of alcohol used • VR setting for reflux • VR setting for distillation • Theoretical yield calculation • % yield calculation • Physical state and color of product • GC vial slot # • Give an example of an adjusted area % calculation

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