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LABORATORY NOTEBOOK (Pre-lab). OBJECTIVE ( Must clearly state…) What compounds you will make and how How you will purify the compound How you will determine the purity of your compound CHEMICAL EQUATION Include the general chemical equation from top of page 93 .
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LABORATORY NOTEBOOK(Pre-lab) • OBJECTIVE (Must clearly state…) • What compounds you will make and how • How you will purify the compound • How you will determine the purity of your compound • CHEMICAL EQUATION • Include the general chemical equation from top of page 93. • TABLE OF PHYSICAL DATA (Single organized table, must include...) • LIQUIDS: (MW, bp, density, hazards) 2-methylcyclohexanol, Hydrobromic acid, sulfuric acid, 1-bromobutane, 2-bromobutane, 2-bromo-2-methylpropane, 1-bromo-1-methylcyclohexane (no bp/density required), and 1-bromo-2-methylcyclohexane (no bp/density required). • REFERENCE TO PROCEDURE (Must include…) • full title • Edition • authors • page numbers where actual procedure can be found
LABORATORY NOTEBOOK(In-lab) • DATA/CALCULATIONS • Initial weight of 2-methylcyclohexanol used • Initial 50 mL beaker weight • Final 50 mL beaker weight • Final product weight • Physical state and color of product • Theoretical yield calculation (not just the number!) • Percent yield calculation (not just the number!) • EXPERIMENTAL PROCEDURE • In paragraph form, describe the procedure that you actually followed during the lab. • Paragraph must be written in PAST TENSE, PASSIVE VOICE. • Include ACTUAL volumes or weights of chemicals used during the experiment. • Include any mistakes, accidents, or observations if necessary.