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LABORATORY NOTEBOOK (Pre-lab). TITLE AND DATE OBJECTIVE CHEMICAL EQUATION AND MECHANISM Include the chemical equation from the top of page 199 and the complete mechanism from page 200. TABLE OF PHYSICAL DATA
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LABORATORY NOTEBOOK(Pre-lab) • TITLE AND DATE • OBJECTIVE • CHEMICAL EQUATION AND MECHANISM • Include the chemical equation from the top of page 199 and the complete mechanism from page 200. • TABLE OF PHYSICAL DATA • Include physical constants and hazards for 3,4-dimethoxybenzaldehyde, 1-indanone, sodium hydroxide, ethanol, diethyl ether, and hexane. • PRE-LAB CALCULATION • Include theoretical yield calculation for the reaction. • PROCEDURE • Include a reference to the lab manual pages where the actual procedure can be found.
LABORATORY NOTEBOOK(In-lab) OBSERVATIONS/CALCULATIONS MUST INCLUDE, BUT NOT LIMITED TO: • Weights of aldehyde, ketone, and NaOH used • Volume of 90:10 propanol/water used for recrystallization • Weight of filter paper • TLC diagram • Atom economy calculation • Experimental atom economy calculation • E product calculation • Cost per gram calculation