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Novel crystallite carbon based on Mesophase -pitch. December 8, 2011. Contents. BGBU The Structure for Novel Crystallite Carbon Some Questions. Building from Granular Basic Units (BGBU). The precursor of the novel crystallite carbon. Thermal polycondensation. Stacking.
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Novel crystallite carbon based on Mesophase-pitch December 8, 2011
Contents BGBU The Structure for Novel Crystallite Carbon Some Questions
The precursor of the novel crystallite carbon Thermal polycondensation Stacking Pitch molecules BBU of mesophase pitch Mesophase molecule
Yellow dot —the light components in the matrix Basic units Growing trend Three-dimensional structure Novel Crystallite Carbon ? activation carbonization
Stabilization of the mesophase pitch Coal-tar pitch Coal-tar pitch oxygen atom will be brought in Oxidation in the air Delayed coking The product contains many macropores Precursor Precursor
Experiments Coal-tar pitch Temperature and time Controlling Thermal condensation Mesophase pitch Fig.1 Reaction equipment. 1、3. Thermocouples 2. Pressure gauge 4、6. Valve 5. Heating furnace 7. Reaction vessesl 8. Stirring paddle Fig.2 the flowchat of the experiments
Results CTP: coal-tar pitch CTP-360-6: heat treatment at 360℃ for 6 hours CTP-410-0.5: heat treatment at 410℃ for 30min SP: softening point TI: toluene insolubles QI: quinoline insolubles
questions • How to control the conditions of the preparation for the proper precursors? • Some others appropriate methods for the stabilization of the mesophase pitch?